摘要
从中国广西药用植物苍白秤钩风 (Diploclisiaglaucescens)藤茎的 95 %乙醇提取物中分离得到 5个脱皮甾酮类化合物 ( 1 5 )。通过NMR、MS以及化学沟通等方法分别将其结构鉴定为 paristeroneC 2 0 ,2 2 monoacetonide( 1) ,paristerone( 2 ) ,ecdysterone( 3) ,makisteroneC( 4 )和capisterone( 5 )。化合物 1为首次从自然界分得的天然产物 ,2 ,4 。
Five ecdysteroids were isolated from the EtOH extract of the stems of Diploclisia glaucescens. Their structures were identified as paristerone 20,22 monoacetonide(1),paristerone(2),β ecdysterone(3),makisterone C(4)and capitasterone(5),respectively,on the basis of chemical and physical evidence.This is the first report of paristerone 20,22 monoacetonide isolated from natural source.Compounds 2,4,and 5 were also isolated for the first time from D.glaucescens .
出处
《天然产物研究与开发》
CAS
CSCD
2003年第2期93-97,共5页
Natural Product Research and Development
基金
ThisresearchissupportedbyNationalScienceFoundationforOutstandingYouth(30125044)andthe"FoundationforScholarsComeBackfromAbroad"providedbyMinistryofEducation,MinistryofPersonnel,andChineseAcademyofSciences
关键词
苍白秤钩风
脱皮甾酮类
化学成分
结构鉴定
天然产物
药用植物
Menispermaceae
Diploclisia glaucescens
ecdysteroid
paristerone 20,22 monoacetonide
paristerone
ecdysterone
makisterone C
capitasterone