2,5-二甲氧基-4-吗啉基苯基重氮氯化锡复盐的合成

2,5-DIMETHOXY-4-MORPHOLINO BENZENEDIAZONIUM CHLORIDE SnCl_4 COMPLEX

本文采用较为简便的合成手段,较好地合成了一种高速感光重氮型化合物--2,5-二甲氧基-4-码啉基苯基重氮氯化锡复盐,并经 IR 谱、′HNMR 谱,以及元素分析等检测,证实该产物的存在.产品紫外特征吸收峰艾λ_(max)=398. 2nm,热分解温度为158℃.

In this paper,a kind of superfast photosensitire diazo agent,2,5-dimethoxy-4-morpholino enzenediazonium chloride SnCl_4 complex,is prepared.We measure IR spectra,'HN-MR spectra and UV-VIS spectra of the diazo double salt,and also the analysis of elements.These methods can prove the existence of the product.The diazonium group characteristic absorption peak of UV-VIS spectra is 398. 2nm and the temperature of decomposition is 158℃.