用脱叔丁基法制备不对称3,3’,5-三叔丁基-4,4’-联苯醌的合成条件研究

Study on synthesis of 3,3', 5-tributyl-4, 4'-dibenzoquinone through debutylation

对用脱叔丁基的方法合成标题化合物的合成条件进行了讨论和研究,优化了其氧化、脱叔丁基的反应条件,使目标产物的总体产率由文献的9％提高到15％。

In this paper, better conditions of oxidation and debutylation are introduced to prepare 3, 3', 5-tributyl-4, 4 -dibenzoquinone. The yields of products are improved.