摘要
介绍了4-(一氯、二氯、三氯)代乙酰基安替比林的合成(产率分别为26%、56%、46%)及其熔点、溶解性;还进行了元素分析、X-射线衍射、质谱、紫外光谱和红外吸光谱等的测试。
In this paper,a new method of synthesizing4-(monochloro,dichloro,trichloro)acetylanti-pyrine is recommended.Their compositions weredetermined by elemental analysis and mass spec-tra.Their melting point,solubility in differentsolvents,X-ray powder diffraction,ultraviolet andinfrared spectra were also studied.
出处
《化学试剂》
CAS
CSCD
北大核心
1992年第3期175-176,192,共3页
Chemical Reagents
基金
国家自然科学基金