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六氰合铁酸铜钴薄膜修饰电极的in-situ FTIR研究 被引量：1

In-situ FTIR Study of Hybrid Copper-cobalt Hexacyanoferrate Film Modified Electrode
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摘要 本文用循环伏安法在铂电极的表面电沉积了六氰合铁酸铜钴薄膜 ,结合电化学方法 ,研究了修饰膜氧化过程中的现场红外光谱。 The study on the in-situ FTIR spectroelectrochemistry of a hybrid copper-cobalt hexacyanoferrate film modified platinum electrode was carried out. The variation of the FTIR spectra was well correlated to the redox process of CuCOHCF. The relative contribution of Cu(II) and Co(II) to the stretching vibration of CN was found to vary with the applied potential.
作者 崔兴品 汪夏燕 林祥钦
机构地区 中国科学技术大学化学系
出处 《光谱学与光谱分析》 SCIE EI CAS CSCD 北大核心 2003年第3期603-604,共2页 Spectroscopy and Spectral Analysis
基金 国家自然科学基金 (No 2 0 0 750 2 5)资助课题
关键词 六氰合铁酸铜钴薄膜 修饰电极 in-situFTIR 电化学 红外光谱 铂电极 导电聚合物 hybrid copper-cobalt hexacyanoferrate in-situ FTIR spectroelectrochemistry
分类号 O657.1 [理学—分析化学]
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参考文献11

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同被引文献20

  • 1刘少琼,黄河,熊予莹,于黄中,任斌.PANI/TiO_2和PANI/TiO_2/HCSA纳米复合材料的光电性能[J].半导体光电,2002,23(1):57-60. 被引量：3
  • 2蒋静,李良超,徐烽,颜冲.聚苯胺-LiNi铁氧体复合纳米微粒的原位合成及其键合机制[J].化学学报,2007,65(1):53-58. 被引量：17
  • 3Wang Z Z,Bi H, Liu J. Magnetic and microwave! absorbing properties of polyaniline/'γ-Fe^2O^3 nanoeomposite [J]. J Magn Magn Mater, 2008, 320(16): 2132.
  • 4Subramania A, Subbarao L D. Polyaniline nanofibers by surfactant-assisted dilute polymerization for supercapacitot applications[J]. Polym Adv Technol, 2008, 19(7) : 725-727.
  • 5Orata D,David S K. A comparative study of the electroehemical/e!ectro-degradation of polyaniline from aniline loaded in a elay-mineral/polyaniline composite matrix to that of the bulk solution [J]. React Funct Polym, 2000,43(1):133-138.
  • 6Orata D, Segor F. Electrodeposition of polyaniline on acidified clay montmorillonite modified electrode [J]. React Funtl Polym,2000, 43(3) : 305.
  • 7de Tacconi N R,Rajeshwar K,Lezna R O. Metal hexacyanoferrates: Electrosynthesis, in situ characterization, and applications [J]. Chemistry of Materials, 2003, 15 (16) .. 3046-3062.
  • 8Prabakar Richard S J,Narayanan S. Flow injection analysis of BHA by NiHCF modified electrode [J]. Food Chem,2010, 118: 449-455.
  • 9Kulesza P J,Miecznikowski K, Malik M A,et al. Electrochemical preparation and characterization of hybrid films composed of Prussian blue type metal hexacyanoferrate and conducting polymer [J]. Electrochim Acta, 2001, 46: 4065-4073.
  • 10Milczarek G. Self-doped polyaniline films prepared by electropolymerization in the presence of sulfonated nickel phthalocyanine [J]. Thin Solid Films, 2009, 517: 79- 84.

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光谱学与光谱分析
2003年 第3期

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