摘要
由2—甲氧基—5—芳偶氮基革酮与芳胺直接缩合反应制备了一系列新的2—芳胺基—5—芳偶氮基革酮化合物(6a-i),用^1H-NMR和元素分析表征了结构。通过差示扫描量热法研究了其热力学性质,并结合分子结构进行了探讨。
A series of new 2-arylamino-5-arylazotropones(6a-i) were prepared by condensating 2 - methoxyl - 5 - arylzaotropones and substituted anilline. The structures we,re determined by 1H-NMR and Element - Analyst. Their thermodynamics properties were studied by Different Scanning Calorimetry, and discussed on their molecular structure.
出处
《延边大学学报(自然科学版)》
CAS
2003年第2期107-110,156,共5页
Journal of Yanbian University(Natural Science Edition)