微波诱导清洁合成高纯碘酸钾研究

Study on the Clean Synthesis of High - Pure Potassium lodate by Microwave Irradiation

利用微波诱导,用清洁氧化剂过氧化氢氧化碘合成了高纯碘酸钾。最佳合成条件:过氧化氢与碘的摩尔比5.4:1,微波辐射时间12min,微波功率600W,产率94.6％。

The clean synthesis of potassium iodate was performed by oxidation of ozogen. The optimum synthetic conditions were as follows: the ratio of ozogen to iodine was 5.4:1, microwave irradiation time was 12 min, microwave power was 600 W. Under such synthetic conditions,the yield was up to 94.6 %.