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椭球形α-Fe_2O_3纳米薄膜的制备与气敏性能 被引量:3

Preparation and Gas-sensing Property of Ellipsoidal Shaped α-Fe_2O_3 Nano-films
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摘要 The α Fe 2 O 3 sol was prepared by a sol gel method from FeCl 3 ·6H 2 O. Thin nano particulate films of the α Fe 2 O 3 were deposited on glass substrate by dip coating sol gel technique. The structure and morphology of the thin films were characterized by XRD, UV Vis and AFM analysis methods. The XRD results revealed that the nano crystal with (104) preferential orientation has been formed on glass substrate. The UV Vis spectra showed that the nano particulate films obtained from Fe 2 O 3 aqueous colloidal sols are well transferred to glass substrate at dip coating rate of 80 mm/min. The α Fe 2 O 3 particles are ellipsoidal shaped, with particle size of about 5~7 nm. The multilayer films exhibited high sensitivity to ethanol vapor at room temperature. The α Fe 2 O 3 sol was prepared by a sol gel method from FeCl 3 ·6H 2 O. Thin nano particulate films of the α Fe 2 O 3 were deposited on glass substrate by dip coating sol gel technique. The structure and morphology of the thin films were characterized by XRD, UV Vis and AFM analysis methods. The XRD results revealed that the nano crystal with (104) preferential orientation has been formed on glass substrate. The UV Vis spectra showed that the nano particulate films obtained from Fe 2 O 3 aqueous colloidal sols are well transferred to glass substrate at dip coating rate of 80 mm/min. The α Fe 2 O 3 particles are ellipsoidal shaped, with particle size of about 5~7 nm. The multilayer films exhibited high sensitivity to ethanol vapor at room temperature.
出处 《应用化学》 CAS CSCD 北大核心 2003年第8期794-796,共3页 Chinese Journal of Applied Chemistry
基金 国家自然科学基金 ( 2 0 10 10 0 3 ) 黑龙江省高校骨干教师创新计划 黑龙江省青年攻关基金 (QC0 2C41)
关键词 Α-FE2O3 纳米薄膜 气敏特性 Fe 2 O 3 ,nano films,gas sensing property
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