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Electrochemical Deposition of Ni-W Gradient Deposit and Its Structural Characterization

Electrochemical Deposition of Ni-W Gradient Deposit and Its Structural Characterization
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摘要 The Ni-W gradient deposit with nano-structure was prepared by an electrochemical deposition method.X-ray diffraction (XRD) and energy dispersive X-ray analysis (EDXA) indicate that the crystallite size of the deposit decreases from 10.3nm to 1.5nm and the crystal grating aberrance increases with the increase of W content in the growing direction of the deposit. The structure of deposit changes from crystalline to amorphous stepwise with associated increase of crystal grating aberrance, and presents gradient distribution. These show that the deposit isgradient with nano-structure. The Ni-W gradient deposit with nano-structure was prepared by an electrochemical deposition method. X-ray diffraction (XRD) and energy dispersive X-ray analysis (EDXA) indicate that the crystallite size of the deposit decreases from. 10.3nm to 1.5nm and the crystal grating aberrance increases with the increase of W content in the growing direction of the deposit. The structure of deposit changes from crystalline to amorphous stepwise with associated increase of crystal grating aberrance, and presents gradient distribution. These show that the deposit is gradient with nano-structure.
出处 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2003年第3期348-351,共4页 中国化学工程学报(英文版)
基金 Supported by the National Natural Science Foundation of China (No.59671058)
关键词 电化学沉积 NI-W合金 结构表征 功能梯度材料 镀层 纳米结构 制备 X-射线衍射 electrochemical deposition, Ni-W alloy, FGM, amorphous
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