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Synthesis and Crystal Structure of an Infinite 1D Zigzag Chain Compound (dimbH^+)(ClO_4^-) and Its Comparison with (dimb)2H_2O (dimb = 1,3-Di(imidazol-1-ylmethyl)-5-methylbenzene)

Synthesis and Crystal Structure of an Infinite 1D Zigzag Chain Compound (dimbH^+)(ClO_4^-) and Its Comparison with (dimb)2H_2O (dimb = 1,3-Di(imidazol-1-ylmethyl)-5-methylbenzene)
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摘要 A new imidazolium compound, C15H17N4ClO4, was prepared from a flexible bidentate ligand of 1,3-di(imidazol-1-ylmethyl)-5-methylbenzene, and characterized by X-ray analysis. It is of orthorhombic, space group Pnma with a = 8.182(2), b = 12.874(3), c = 15.611(4) ? V = 1644.4(7) 3, Dc = 1.425 g/cm3, Z = 4, Mr = 352.78, m(MoKa) = 0.944 mm-1, F(000) = 736, S = 1.036, the final R = 0.0521 and wR = 0.1187 for 1128 observed reflections (I > 2s(I)). An infinite one-dimensional zigzag chain is formed by NH…N hydrogen bonding interactions between the imidazolium salt cations.
作者 YAOJing-Cai MAYong-Lin HUANGWei GOUShao-Hua
机构地区 DepartmentofChemistry CoordinationChemistryInstitute
出处 《Chinese Journal of Structural Chemistry》 SCIE CAS CSCD 北大核心 2003年第4期439-443,共5页 结构化学（英文）
基金 the Natural Science Foundation of Jiangsu province (Grant No Bk2001031)
关键词 di(imidazol-1-ylmethyl)-5-methylbenzene imidazolium salt hydrogen bonding interactions zigzag chain crystal structure 合成 晶体结构 锯齿形链化合物 氮氢键 1,3-双(咪唑-l-甲基)-5-甲苯 咪唑嗡盐 交互作用 超分子化合物
分类号 O626.23 [理学—有机化学] O641.3 [理学—物理化学]
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  • 1Shen, H. Y.; Liao, D. Z.; Jian, Z. H.; Yah, S.P.; Wang, G. L.; Yao, X. K.; Wang, H. G. Acta Chem. Scand. 1999, 53, 387-390.
  • 2Fei, B. L.; Sun, W. Y.; Zhang, Y. A.; Yu, K. B.; Tang, W. X. J. Chem. Soc., Dalton Trans. 2000, 2345-2348.
  • 3Sui, B.; Li, D. E; Fan, J.; Sun, W. Y. Chine.ve Z Inorg. Chem 2002, 18, 83-86;.
  • 4Sun, W. Y.; Fall, J.; Okamut,.a, T. A.; Ueyama, N. Inorg.Chem. Comm 2000, 3, 541-544;.
  • 5Li, B.; Yao, J. C.; Gou, S. H. (in press).
  • 6Liu, H. K.; Sun, W. Y.; Zhu, H. L.; Yu, K. B.; Tang, W. X. Inorg. Chim. Acta 1999, 295, 129-135;.
  • 7Cai, Y. P.; Kang, B. S.; Su, C. Y.; Zhang, H.X., Yang, X. P., Deng, L. R., Xu, A. W.; Zhou, Z. Y. Chinese J. Struct. Chem. 2001, 20, 262-265.
  • 8Yamagiwa, Y.; Koreishi, Y. Kiyozumi, S.; Kobayashi, M.; Kamikawa, T. Bull. Chem. Soc. Jpn. 1996, 69, 3317-3323.
  • 9Hoskins, B. F.; Robson, R., Slizys, D. A. Angew. Chem., Int. Ed. Engl. 1998, 36, 2752-2755.
  • 10Dhal, P. K.; Arnold, E H. Macromolecules 1992, 25, 7051-7059.
Chinese Journal of Structural Chemistry
2003年 第4期

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