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微波消解石墨炉原子吸收光谱法测定番木瓜酱菜中铅 被引量:8

GF-AAS DETERMINATION OF LEAD IN PICKLED PAPAYA——DIGESTION OF SAMPLE BY MICROWAVE-HEATING
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摘要 研究了微波消解石墨炉原子吸收光谱法测定番木瓜酱菜中铅的最佳条件 ,方法简便快速 ,检出限为 0 .0 6 8mg·kg- 1(换算到样品中的最终浓度 ) ,RSD为 1.4 %~ 9.6 % ,样品加标回收率为97.7%~ 10 0 .3%。 Conditions for the GF-AAS determination of microamounts of lead in pickled papaya, including the acid-digestion of sample by microwave-heating, the working parameters of the instrument, elimination of the interference of sodium chloride and etc, were studied and optimized. The limit of detection of this method was found to be 0.068mg·kg -1 , RSD′s found were in the range of 1.4%~9.6%, and recoveries were in the range of 97.7%~100.3%.
作者 康远干
出处 《理化检验(化学分册)》 CAS CSCD 北大核心 2003年第7期391-392,共2页 Physical Testing and Chemical Analysis(Part B:Chemical Analysis)
关键词 微波消解 石墨炉原子吸收光谱法 测定 番木瓜酱菜 食品卫生 GF-AAS Microwave heating Acid digestion of sample Lead Pickled papaya
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  • 1.SB/T10217—1994.中华人民共和国行业标准-酱油渍菜[S].,1994..
  • 2陈怀庆 梁声记 等.番木瓜系列食品的开发研究[J].广西热作科技,1987,(2):17-23.

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