摘要
以间甲酚为原料,经乙酰氧化,氯化成乙酰氧基氯苄和乙酰氧基氯化亚苄的混合物,然后使用Sommelet反应合成间羟基苯甲醛,优化了工艺条件,其收率(基于间甲酚)可达70%。
m-Hydrobenzaldehyde was prepared by m-cresol as raw material ,by acetoxying and chloriding to give mix that comprise acetoxybenzylchloride and acetoxybenzyene chloride. By Sommelet reaction, optimized technics qualification was obtained , the translation of m-cresol was 70%?
出处
《河北化工》
2003年第4期22-23,共2页
Hebei Chemical Industry
