凝胶制品中合成着色剂分析的样品前处理方法改进

Improved method for sample pretreatment on detecting synthetic coloring agents in colloid products

目的对凝胶制品中4种合成着色剂柠檬黄、日落黄、苋菜红、胭脂红检测的样品前处理方法进行改进。方法以国家标准GB/T 5009.35-2003规定的样品前处理方法为依据,进行合成着色剂分析样品前处理方法的改进。结果结果表明提取方法改进后可明显提高凝胶制品中4种着色剂的提取效率。结论本法处理样品时,解析分离步骤易于进行,改变样品的预处理条件后,其准确度、精密度仍很高,重现性均符合分析要求,可应用于实际检测工作中。

Objective To improve the method of sample pretreatment on detecting 4 kinds of synthetic coloring agents, including tartrazine, sunset yellow, amaranth and new coccine in colloid products.Methods Based on GB/T 5009.35-2003Determination of synthetic colour in foods, sample pretreatment of the synthetic coloring agents was improved.Results It showed that the improved method could obviously enhance extraction rate of 4 kinds of coloring regents in colloid products, compared with GB/T 5009.35-2003. Conclusion Using the improved method, the analytical separate steps can be carried out easily in sample treating, and this method has the advantages of accuracy, precision and high reappearance for the determination of synthetic coloring agents in practical work.