期刊文献+
任意字段
题名或关键词
题名
关键词
文摘
作者
第一作者
机构
刊名
分类号
参考文献
作者简介
基金资助
栏目信息

海星甾醇的分离精制与测定 被引量：1

THE SEPARATION AND DETERMINATION OF STEROLS IN STARFISH(Asterias amurensis)
下载PDF
导出
摘要 采取甲醇多步结晶法 ,从海星(Asteriasamurensis)中分离精制了海星甾醇。利用高效液相色谱 ,对海星甾醇中的胆甾醇含量进行了测定。研究结果表明 ,在选定的色谱条件下 ,胆甾醇测定结果线性良好 ,精密度好 ,准确度高。 Multilevel fractional crystallization was used to separate sterols from Starfish(Asterias amurensis),and the content of cholesterol was determined by HPLC.Under selected chromatography conditions,the cholesterol can be determined accuˉrately and rapidly.The result shows this proposed method has provided a reference basis for making the quality control standards for cholesterol from Starfish(Asterias amurensis).
作者 文震 党志 朱志鑫 李琼
机构地区 华南理工大学应用化学系
出处 《海洋科学》 CAS CSCD 北大核心 2003年第9期61-64,共4页 Marine Sciences
基金 教育部高等院校博士点基金项目20020561026号 广东省自然科学基金资助
关键词 海星甾醇 分离 精制 测定 海洋生物 Sterols,Cholesterol,Starfish(Asterias amurensis),HPLC,Separation
分类号 Q548.1 [生物学—生物化学]
  • 相关文献

参考文献8

  • 1张蓉真,李珑,刘树滔,陈儒明,饶平凡.测定鸡蛋胆固醇的高效液相色谱新方法[J].色谱,1998,16(2):91-94. 被引量：35
  • 2高瑜莹,裘爱泳,潘秋琴,史小华.植物甾醇的分析方法[J].中国油脂,2001,26(1):25-28. 被引量：48
  • 3刘红兵,展翔天,顾谦群,管华诗.近三年我国海洋中药研究进展[J].中国海洋药物,1999,18(4):29-32. 被引量：7
  • 4Shahidi Nasrollah T. A review of the chemistry, biological action, and clinical applications of anabolic-androgenic steroids. Clinical Therapeutics, 2001, 23(9) : 1 355-1 390.
  • 5Kicha A A,Ivanchina N V, Gorshkova I A, et al. The distribution of free sterols, polyhydroxysteroids and steroid glycosides in various body components of the starfish Patiria( = Asterina) pectinifera. Comparative Biochemistry and Physiology, Part B, 2001, 128:43-52.
  • 6Iorizzi M, De Marino S, Minale L, et al. Investigation of the polar steroids from an Antarctic Starfish of the family Echinasteridae : isolation of twenty seven polyhydroxysteroids and steroidal oligoglycosides, structures and biological activities. Tetrahedron, 1996, 52(33) : 10 997-11 012.
  • 7Abidi S L. Chromatographic analysis of plant sterols in foods and vegetable oils, Chromatography A, 2001,935 : 173-201.
  • 8Shimada K, Mitamura K, Higashi T. Gas chromatogaphy and high-performance liquid chromatography of natural steroids.Journal of Chromatography A, 2001,935 : 141-172.

二级参考文献61

共引文献84

同被引文献23

  • 1曹莹,谷克仁,孟冬,茹湘波.植物甾醇提取方法研究进展[J].粮油食品科技,2006,14(5):25-28. 被引量：27
  • 2Lockwood G B, Brain K R. Simultaneous estimation of sterol and steroidal sapogenin in plant extracts by densit- ometrie thin- layer chromatographyJJ. Journal of Chromatography , 1974,95 : 250 - 253.
  • 3Guoqiang Li, Zhiwei Deng, Huashi Guan, et al. Ster- oids from the soft coral Dendronephthya sp. E J J- Ster- oids,2005,70:13- 18.
  • 4Changyih Duh, Iwen Lo, Shangkwei Wang, et al. New cytotoxic steroids from the soft coral Clavularia viridis [J]. steroids, 2007,72 : 573 - 579.
  • 5Yaching Huang, Zhihong Wen, Shangkwei Wang, et al. New anti- inflammatory 4 - methylated steroids from the Formosan soft coral Nephthea chabroli [J]. Steroids,2008,73 : 1181 - 1186.
  • 6Efstathia Ioannou, Ayman F Abdel- Razik, Maria Zervou, et al. 5a, 8a- Epidioxysterols from the gor- gonian EuniceIla cavolini and the ascidian Trididem- hum inarmatum Isolation and evaluation of their anti- proliferative activity[J]. Steroids, 2009,74 . 73 - 80.
  • 7Efstathia Ioannou, Ayman F Abdel- Razik, Xanthippi Alexi, et al. 9, 11 - Secosterols with anti - prolifera- tive activity from the gorgonian. Eunieella cavolini[J]. Bioorganic Medicinal Chemistry, 2009 , 17 : 4537 -4541.
  • 8Xiaohong Yan, Liping Lin, Jian Ding, et al. Methyl spongoate, a cytotoxic steroid from the Sanya soft cor- al Spongodes sp. [-JJ. Bioorganic Medicinal Chemis- try Letters, 2007,17:2661-2663.
  • 9Ana Rueda, Eva Zuh'a, Mara J Orteg'a, et al. Struc- ture and cytotoxicity of new polyhydroxylated sterols from the Caribbean gorgonian Plexaurella grisea [J]. Steroids,2001, 66:897 - 904.
  • 10Shiyie Cheng, Changfeng Dai, Changyih Duh. New 4 - methylated and 19 - oxygenated steroids from the Formosan soft coral Nephthea erecta [J 7. Steroids, 2007,72:653 - 659.

引证文献1

二级引证文献3

海洋科学
2003年 第9期

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部