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水热法合成掺杂铁离子的小管径TiO_2纳米管 被引量:31

Preparation of Fe-doped TiO2 Nanotubes with Small Diameter by Hydrothermal Method
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摘要 Using Fe doped titania powders as the precursor, Fe doped TiO2 nanotubes with small diameter of 10nm were obtained by hydrothermal method. The doped titania powders have two different crystalline phases, anatase and rutile of which the average particle diameters are 30.3nm and 41.7nm, receptively. The products were characterized by TEM, XRD and EDS. The results showed that Fe doped TiO2 nanotubes of 200nm in length could be obtained from Fe doped rutile powder, and have higher yields. The formation mechanism of long titania nanotubes was suggested in the light of the relative stability of crystalline phase. Using Fe-doped titania powders as the precursor, Fe-doped TiO2 nanotubes with small diameter of 10 nm were obtained by hydrothermal method. The doped titania powders have two different crystalline phases, anatase and rutile of which the average particle diameters are 30.3 nm and 41.7 nm, receptively. The products were characterized by TEM, XRD and EDS. The results showed that Fe-doped TiO2 nanotubes of 200 nm in length could be obtained from Fe-doped rutile powder, and have higher yields. The formation mechanism of long titania nanotubes was suggested in the light of the relative stability of crystalline phase.
机构地区 浙江大学化学系
出处 《无机化学学报》 SCIE CAS CSCD 北大核心 2003年第8期899-901,共3页 Chinese Journal of Inorganic Chemistry
基金 国家自然科学基金资助项目(No.20171039 50171036) 浙江省自然科学基金资助项目(No.200053)
关键词 水热法合成 掺杂 铁离子 小管径 TIO2 纳米管 二氧化钛 hydrothermal method titania doping nanotube
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