期刊文献+

水溶性光疗药物TPPS_4的合成及提纯的研究 被引量:1

Study on the Purification of Tetra-(P-Sulfonatophenyl)Porphyrin Tetrasodium Salt
下载PDF
导出
摘要 研究旨在改进光疗药物水溶性四(对磺酸钠苯基)卟啉(TPPS4)的合成方法,特别是产物的提纯方法。以四苯基卟啉为原料,经氯磺酸或浓硫酸处理合成TPPS4,然后进行以渗析和萃取分液为主的后处理。 The method of purifing tetra(psulfonatophenyl)porphyrin tetrasodium salt is developed. The title compound is synthesized by reaction of tetraphenyl porphyrin with chlorosulfonic acid or concentrated sulphuricacid. Postpurification process of the product consists of extraction with butanol and dialysis in a semipermeable membrane.
作者 陈阳 马金石
出处 《武汉科技大学学报》 CAS 2003年第3期254-255,共2页 Journal of Wuhan University of Science and Technology
关键词 四(对磺酸钠苯基)卟啉 合成 提纯 tetra-(p-sulfonatophenyl)porphyrin tetrasodium salt synthesis purification
  • 相关文献

参考文献5

二级参考文献7

共引文献51

同被引文献9

  • 1赵春杰,黄东萍,张仲元,佟志清,李长见.HPLC同时测定人血清和人发中微量铬锌铜铅的含量[J].中国药学杂志,1995,30(3):162-165. 被引量:12
  • 2黎先超,胡景,孙小梅.原卟啉-吐温80-硫酸铵液固体系分离和测定铜、镍的研究[J].冶金分析,2006,26(3):72-74. 被引量:4
  • 3Manfred Doss.Conversion of porphyrin methyl esters to zinc and copper chelates for spectrophotometric analysis[J].Analytical Biochemistry,1971,39 (1):7-14.
  • 4Amit Chatterjee,Hiroaki Tao,Yasuyuki Shibata.Determination of selenium compounds in urine by high-performance liquid chromatography-inductively coupled plasma mass spectrometry[J].Journal of Chromatography A,2003,997(1-2):249-257.
  • 5Shi Zhihong,Fu Chengguang.Porphyrins as ligands for trace metal analysis by high-performance liquid chromatography[J].Talanta,1997,44(4):593-604.
  • 6Hu Qiufen,Yang Guangyu,Li Haitao,et al.Study on determination of seven transition metal ions in water and food by microcolumn high-performance liquid chromatography[J].Bulletin of Korean Chemical Society,2004,25 (5):694-698.
  • 7Yuichiro Kashiyama,Hiroshi Kitazato,Naohiko Ohkouchi.An improved method for isolation and purification of sedimentary porphyrins by high-performance liquid chromatography for compound-specific isotopic analysis[J].Journal of Chromatography A,2007,1138(1-2):73-83.
  • 8丁学军.meso-四对磺酸苯基卟啉的合成[J].化学世界,1990,31(4):164-166. 被引量:5
  • 9张松,潘超,乔庆东.四苯基卟啉及其衍生物的合成和可见光谱的研究[J].化工科技,2003,11(5):15-17. 被引量:9

引证文献1

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部