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Synthesis ofγ-MnOOH nanorods by successive ionic layer deposition method and their capacitive performance 被引量:3

Synthesis of γ-MnOOH nanorods by successive ionic layer deposition method and their capacitive performance
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摘要 It was first shown in the present study that layers of manganite γ-Mn OOH can be deposited on the surface of a substrate by its multiple successive treatment by the solutions of MnSO;and K;S;O;using the successive ionic layer deposition(SILD) technique. Their analysis was carried out by the XRD, XPS, FT-IR,SEM and EDX methods. It has shown that the synthesized layers are formed by aggregates of nanorods up to 80–100 nm in length and approximately 8–10 nm in diameter. A probable sequence of chemical reactions leading to the formation of a layer of the given morphology is suggested. Testing of performance of supercapacitors with nickel foam electrodes incorporating the γ-Mn OOH layers in the 0.1 M KOH electrolyte at 1 A/g indicated the specific capacitance equal to 1120 F/g. After 1000 work cycles the observed degradation of this value was less than 3%. It was first shown in the present study that layers of manganite γ-Mn OOH can be deposited on the surface of a substrate by its multiple successive treatment by the solutions of MnSO_4 and K_2S_2O_8 using the successive ionic layer deposition(SILD) technique. Their analysis was carried out by the XRD, XPS, FT-IR,SEM and EDX methods. It has shown that the synthesized layers are formed by aggregates of nanorods up to 80–100 nm in length and approximately 8–10 nm in diameter. A probable sequence of chemical reactions leading to the formation of a layer of the given morphology is suggested. Testing of performance of supercapacitors with nickel foam electrodes incorporating the γ-Mn OOH layers in the 0.1 M KOH electrolyte at 1 A/g indicated the specific capacitance equal to 1120 F/g. After 1000 work cycles the observed degradation of this value was less than 3%.
出处 《Journal of Energy Chemistry》 SCIE EI CAS CSCD 2017年第3期336-339,共4页 能源化学(英文版)
关键词 MANGANITE NANOLAYERS SILD SUPERCAPACITOR Manganite Nanolayers SILD Supercapacitor
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