摘要
用对硝基苯乙酮、乙二醇、苯乙腈、氢气、高氯酸为原料,经酮基保护,环化,催化加氢和消除反应,合成出较高产率的5-乙酰基-2-氨基二苯甲酮。对反应机理作了初步探讨,并用元素分析、IR和1HNMR对其结构进行了表征。
The 5acetyl2aminobenzophenone with high yield was synthesized by using pnitroacetophenone, ethylene glycol, phenylacetonitrile, hydrogen, perchloric acid as raw materials. The reaction mechanism is discussed simply, and the structure of compound is identified by elemental analysis, IR and 1HNMR.
出处
《国防科技大学学报》
EI
CAS
CSCD
北大核心
2003年第5期31-35,共5页
Journal of National University of Defense Technology
基金
国家部委基金资助项目(51307)
