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氨基磺酸盐-硫酸盐混合溶液中锌-锰合金的电沉积(英文) 被引量：1

Electrodeposition of zinc-manganese alloy from sulphamate-sulphate mixed bath
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摘要 本文研究了氨基磺酸盐-硫酸盐混合溶液中锌-锰合金的电沉积机理。实验结果显示,在低电流密度区获得哑光镀层,锰离子的催化析氢作用降低了合金沉积效率.玻璃化炭黑上的伏安试验显示锌沉积过程中的第一个电子转移较慢,阳极溶出伏安试验显示锌合金的异常共沉积导致富锌中间相的产生。 Zinc-manganese alloy deposit was obtained from sulphamate-sulphate bath. At low current density, matte deposits were obtained. The efficiency of alloy deposition was low due to catalytic evolution of hydrogen by manganese ions. Volta-mmetric studies Carried out on glassy carbon revealed that the first electron transfer is slow in the deposition of zinc. Anomalous codeposition of zinc alloy resulted in zinc rich intermediate phase as revealed by the anodic stripping voltammetric studies.
作者 SM Silaimani S John S Sudharsana V S Muralidharan
机构地区 Central Electrochemical Research Institute
出处 《电镀与涂饰》 CAS CSCD 2003年第6期1-6,28,共7页 Electroplating & Finishing
关键词 锌-锰合金电沉积 异常沉积 循环伏安法 玻璃化炭黑 zinc-manganese alloy electrodeposition anomalous deposition cyclic voltammetry glassy carbon
分类号 TQ153.2 [化学工程—电化学工业] TQ153.43 [化学工程—电化学工业]
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参考文献17

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同被引文献11

  • 1覃奇贤.电镀原理与工艺[M].天津：天津科学技术出版社,1993..
  • 2JOHN S,SILAIMANI S M,ANAND V,et al.Zinc-Manganese alloy plating-A critical review[J].Bulletin of Electrochemisty,2002,18(9):407-412.
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  • 5屠振密,沈品华.电镀锌及锌合金[M].北京:机械工业出版社,2001:1-3.
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  • 7SELVAM M,GURUVAIAH S.Electrodeposition of zinc-manganese alloy from sulphate citrate bath[J].Bulletin of Electrochemistry,1989,5(5):352-365.
  • 8SUGIMOTO Y,URAKAWA T,SAGIYAMA M.The electrodepositon behavior of zinc-manganese alloys from the fluoborate bath[C]//Ext Abs 179th Electrochemistry Society Meeting.USA:Washington D C,1991:831.
  • 9符德学,舒余德,苏永祥,田京城.锌锰合金电沉积研究现状[J].电镀与涂饰,2000,19(4):54-56. 被引量：6
  • 10符德学,舒余德,刘长春,李存红.硫酸盐-柠檬酸体系锌锰合金电沉积的研究[J].材料保护,2001,34(4):23-25. 被引量：5

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电镀与涂饰
2003年 第6期

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