摘要
The title compound bis-9-fluorenylmethylphenyl silane (C33H26Si, Mr = 450.63) was synthesized and its structure has been synthesized and determined by X-ray analysis. The crystal is of triclinic, space group P with a = 9.478(1), b = 10.0956(1), c = 13.0243(2) ? a = 92.668(2), b = 90.809(2), g = 99.348(2)? l = 0.71073 ?, m(MoKa) = 0.115 mm-1, V = 1288.1(2) 3, Z = 2, Dc = 1.219 g/cm3 and F(000) = 476. The structure was refined to R = 0.0437 and wR(F2) = 0.0963 for 3346 observed reflections with I>2s(I). X-ray diffraction analysis reveals that the title compound is bis-9-fluorenylmethylphenyl silane.
The title compound bis-9-fluorenylmethylphenyl silane (C33H26Si, Mr = 450.63) was synthesized and its structure has been synthesized and determined by X-ray analysis. The crystal is of triclinic, space group P with a = 9.478(1), b = 10.0956(1), c = 13.0243(2) ? a = 92.668(2), b = 90.809(2), g = 99.348(2)? l = 0.71073 ?, m(MoKa) = 0.115 mm-1, V = 1288.1(2) 3, Z = 2, Dc = 1.219 g/cm3 and F(000) = 476. The structure was refined to R = 0.0437 and wR(F2) = 0.0963 for 3346 observed reflections with I>2s(I). X-ray diffraction analysis reveals that the title compound is bis-9-fluorenylmethylphenyl silane.
