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二苯甲酰-D-酒石酸及其一水盐的合成 被引量:3

The Preparation of Dibenzoyl-d-tartaric Acid and its Monohydrate
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摘要 以D-酒石酸与苯甲酰氯为原料反应合成二苯甲酰-D-酒石酸与其一水盐,两者均为重要的手性拆分剂。
出处 《浙江化工》 CAS 2003年第11期16-16,共1页 Zhejiang Chemical Industry
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  • 1戴立信,陆熙炎,朱光美.手性技术的兴起[J].化学通报,1995(6):15-22. 被引量:57
  • 2吕秀娟,梅璐璐,施小新.手性拆分剂L-二苯甲酰酒石酸和L-二乙酰酒石酸的合成工艺研究[J].精细化工中间体,2005,35(4):12-14. 被引量:10
  • 3李雯,赵君颖,章亚冬,胡国勤,赵文恩.一水合-L-(2R,3R)-(-)-二苯甲酰酒石酸的合成[J].郑州大学学报(工学版),2006,27(2):62-64. 被引量:5
  • 4FEDERSEL H J, JAKSCH P, SANDBERG R. An efficient synthesis of a new, chiral 2', 6' - pipecoloxylidide local anaesthetic agent [J]. Acta Chem Seand, 1987,B41:757 - 761.
  • 5KATALIN N, MARIA A, ZSUZSA M, et al. Study of the diastereoisomers formed between (N - alkyl) - pipecolic acid- anilides and 2R, 3R- tartaric acid or O, O' -dibenzoyl- 2R, 3R - tartaric acid: Do the tartaric acidform molecular - complexes, instead of salts during optical resolutions? [ J ] . Tetrahetron, 1996, 52 ( 5 ) : 1637-1642.
  • 6LING Q, PENG J S . Process for optical resolution method for fexofenadine HC1 salt[ P]. CN: 1442407,2003- 04-11.
  • 7BORGHESE A, LIBERT V, ZHANG T. Efficient fasts creening methodology for optical resolution agents: Solvent effects are used to affect the efficiency of the resolution process [ J ]. Organic Process Research & Development, 2004, 8(3): 532- 534.
  • 8KUDO J, HIRATA N, YOSHIDA T. A process for the preparation of an opticallyactive 4 - (tert - butoxycar-bonyl) piperazine compound[ P] . EP: 1236722, 2002 -09-04.
  • 9KASSAI C, BALINT J, JUVANCZ Z. Isomer and enantiomer separation of 2 - and 4 - alkyl - cyelohexanols by stereoselective complex formation with O, O' - dibenzoyl- (2R, 3R) - tartaric acid[J] . Synthetic Communications, 2001, 31(11) :1715 - 1719.
  • 10BUTLER C L, CRETCHER L H. Preparation of dibenzoyl- d - tartic acid [ J ] . Journal of the American Chemical Society, 1933, 55:2605 - 2620.

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