亚磷酸三哌啶酰胺合成工艺的研究

Study on the synthetic process of tri (pentamethylene) phosphorous triamide

研究了在碱性条件下合成亚磷酸三哌啶酰胺的方法,采用拉丁方格法,对合成的工艺条件进行了 优化和探索.

Tri (pentamethylene) phosphorous triamide was synthesized with PCl3 and piperidine (the molar ratio is 1:7) at 50℃ in organic solvent for 3 h and the yield is 57%.