摘要
用过氧化氢与乙酸酐反应生成过氧乙酸,经Baeyer-Villiger氧化,使环己酮氧化成ε-己内酯,并对其作了IR、MS、1HNMR和元素分析等鉴定。
The reaction between hydrogen peroxide and acetic anhydride produced peracetic acid, then peracetic acid converted cyclohexanone into E-caprolactone by the Baeyer-Villiger oxidation. The synthesized e-caprolactone was identified by IR, MS, HNMR and elemental analysis.
出处
《化学试剂》
CAS
CSCD
北大核心
2003年第6期363-364,共2页
Chemical Reagents
