摘要
以天然锆英石提供Zr源和Si源,采用X射线衍射及扫描电镜等分析手段,研究了钙钛锆石-钙长石(Ca Zr Ti2O7-Ca Al2Si2O8)组合矿物的固相反应合成,初步探讨了Nd、Ce在钙钛锆石-钙长石组合矿物中的固溶。研究表明:采用固相反应工艺获得了钙钛锆石-钙长石组合矿物,最佳合成条件为1250℃保温2 h。
Zirconolite-anorthite(Ca Zr Ti2O7-Ca Al2Si2O8) composite minerals were fabricated by solid-state reaction method using natural zircon which provide Zr and Si source. The samples were characterized by powder X-ray diffraction(XRD) and scanning electron microscopy(SEM) in order to determine the crystalline phases and their microstructures. Nd and/or Ce doped Zirconolite-anorthite composite minerals were also examined. The results show that the optimum synthesis condition is 1250 ℃ for 2 h.
出处
《中国陶瓷》
CAS
CSCD
北大核心
2015年第1期58-61,共4页
China Ceramics
