摘要
目的:建立郁金的灰色关联度模型,评价中山引种郁金样品的质量。方法:鉴于郁金类药材中挥发油和姜黄素为质量标志物(Q-marker),选择醇溶性浸出物、吉马酮、莪术二酮、姜黄素为综合评价指标,测定3个不同品种3个不同产地的72株中山引种郁金样品中的4种主要成分含量,采用灰色关联度法构建中山引种郁金质量的灰色关联度评价模型。结果:72株中山引种郁金样品的相对关联度(γ_i)在0. 262~0. 697,其中10个样品γ_i> 0. 450,37个样品γ_i<0. 300,表明不同产地不同品种的郁金引种后质量存在显著差异。浙江瑞安市马屿镇产的MY-W-4,MY-W-1的γ_i分别为0. 697,0. 525,质量最优。不同产地不同品种的γ_i的平均值在0. 281~0. 420,浙江马屿镇的温郁金样品的γ_i的平均值最大,质量总体水平最高,可作为郁金优质种源引种。结论:基于多指标成分构建的灰色关联度模型评价引种郁金质量,方法简单客观全面,可用于引种郁金质量评价,为优质种源的筛选提供了参考依据。
Objective:To establish the gray relational analysis for quality evaluation of the samples of Curcumae Radix introduced in Zhongshan.Method:With volatile oil and curcumin as Q-markers,and alcohol extract,germacrone,germacr-1(10)-ene-5,8-dione and curcumin as comprehensive evaluation index,the contents of the four main components in 72 samples of Curcumae Radix of 3 different varieties introduced in Zhongshan from 3 different regions were determined.The grey relational method was used to build the gray correlation evaluation model for Curcumae Radix introduced in Zhongshan.Result:The relative correlation degree(γ_i)of 72 samples was between 0.262 and 0.697,in whichγ_i was above 0.450 for 10 samples,and below0.300 for 37 samples,indicating great differences in the quality of Curcumae Radix after introduction.Theγ_iwas0.697 and 0.525 respectively for No.MY-W-4 and No.MY-W-1 from Curcumae Radix in Mayu with the best quality.The average values ofγ_ifor the samples of 3 different varieties from 3 different regions were between 0.281 and 0.420,and Mayu samples had the maximum average value,indicating that Mayu samples had the highest overall quality of,and could be introduced as excellent resources.Conclusion:The evaluation method combined with GRA method and multi-index quantification was simple,objective and comprehensive,and could be used to evaluate the quality of Curcumae Radix introduced in Zhongshan,so as to provide references for screening highquality provenance.
作者
张娜
翁伟锋
黄淳
魏坤盛
吴旖
ZHANG Na;WENG Wei-feng;HUANG Chun;WEI Kun-sheng;WU Yi(Zhongshan Torch Polytechnic,Zhongshan 528436,China;Zhongshan Health Product Center,National Engineering Research Center for Modernization of Traditional Chinese Medicine,Zhongshan 528436,China;Zhuhai College of Jilin University,Zhuhai 519000,China)
出处
《中国实验方剂学杂志》
CAS
CSCD
北大核心
2019年第15期174-184,共11页
Chinese Journal of Experimental Traditional Medical Formulae
基金
2017年广东省普通高校青年创新人才项目(自然科学)(2017GKQNCX083)
2014年度中山市科技计划项目(2014A2FC257)
关键词
中山引种郁金
灰色关联度法
醇溶性浸出物
吉马酮
莪术二酮
姜黄素
Curcumae Radix introduced in Zhongshan
gray relational method
alcohol extract
germacrone
germacr-1(10)-ene-5,8-dio-ne
curcumin