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微弧氧化钛膜的结合强度与生物活性 被引量:20

ADHESIVE STRENGTH AND BIOACTIVITY OF TITANIA FILMS PREPARED BY MICRO-ARC OXIDATION
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摘要 采用微弧氧化在纯钛表面合成了含钙和磷的氧化钛膜。研究了电压对膜微观结构和结合强度的影响,并评价了微弧氧化钛膜的生物活性。结果表明:钛微弧氧化膜呈多孔结构,高电压下(450 V)所制备的氧化膜在模拟体液(simulated body fluid,SBF)中浸泡14 d后表面可诱导磷灰石生成,呈现较好的生物活性,低电压下所制备的氧化膜不具备生物活性;其结合强度虽随电压的增大而减小,但在250~450 V的电压范围内结合强度均高于31.4 MPa。 Titanium dioxide films containing Ca and P on the surface of titanium were prepared by micro-arc oxidation. The effect of micro-arc voltage on the microstructure and adhesive strength of the films was studied, and the bioactivity of the films was also evaluated. The results show that titanium dioxide films obtained from micro-arc oxidation have porous structure and the films prepared at high voltage of 450 V can induce apatite to form on its surface after soaked in simulated body fluid(SBF) for 14 d. These films present good bioactivity. However, the films prepared at lower voltage have no bioactivity. Their adhesive strength reduces with the increase of the voltage, but it is higher than 31.4 MPa in the voltage of 250-450 V.
出处 《硅酸盐学报》 EI CAS CSCD 北大核心 2004年第2期122-126,共5页 Journal of The Chinese Ceramic Society
基金 国家863计划(2002AA326070) 国家自然科学(50001009) 教育部"跨世纪优秀人才培养计划基金(2001年度)资助项目
关键词 徽弧氧化 氧化钛 生物活性 结合强度 Bond strength (chemical) Morphology Porosity Titanium dioxide X ray diffraction analysis
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参考文献10

  • 1憨勇,徐可为.微弧氧化生成含钙磷氧化钛生物薄膜的结构[J].无机材料学报,2001,16(5):951-956. 被引量:60
  • 2薛文彬,邓志威,来永春,陈如意.LY12铝合金微弧氧化的尺寸变化规律[J].中国有色金属学报,1997,7(3):140-143. 被引量:56
  • 3HENCH L L,WILSON J. An Introduction to Bioceramics[M]. Singapore: World Scientific Publishing Co,1993. p181.
  • 4YEOKHIN A L,NIE X, LEYLAND A, et al. Plasma electrolysis for surface engineering[J]. Surf Coat Technol,1999,122: 73-93.
  • 5HAN Yong, HONG Seong-Hyeon, XU Kewei. Synthesis of nanocrystalline titania films by micro-arc oxidation[J]. Mater Lett, 2002,56(5):744-747.
  • 6HAN Yong, HONG Seong-Hyeon, XU Kewei. Porous nanocrystalline titania films by plasma electrolytic oxidation[J]. Surf Coat Technol,2002,154:314-318.
  • 7HAN Yong, HONG Seong-Hyeon, XU Kewei. Structure and in vitro bioactivity of titania-based films by micro-arc oxidation[J]. Surf Coat Technol, 2003,168:249-258.
  • 8KOKUBO T, KUSHITANI H, SAKKA S,et al. Solutions able to reproduce in vivo surface-structure changes in bioactive glass-ceramic[J]. J Biomed Mater Res, 1990,24: 721-734.
  • 9HANAWA T, KONM, DOIH. Amount of hydroxyl radical on calcium-ion-implanted titanium and point of zero charge of constituent oxide of the surface-modified layer [J]. J Mater Sci:Mater Med,1998,9: 89-92.
  • 10PHAM M T, WATZ W, REUTHER H, et al. Ion beam sensitizing of titanium surfaces to hydroxyapatite formation [J]. Surf Coat Technol, 2000,128-129: 313-319.

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