摘要
采用五氟苄基溴 (PFBBr)衍生化和GC -MS分析方法对氟乙酰胺鼠药进行了检验 ,考察和优化了衍生化条件及分析参数等因素 ,线性范围为 2 .5～ 5 0 μg/mL ,相关系数r=0 .998 6 ,血液样品加标平均回收率为 76 .2 % ,测定结果的相对标准偏差为 3.0 7%。
The determination of fluoroactamide by PFBBr pre-column derivation and GC-MS was studied. Derivation conditions and analytical parameters were researched and optimized, the linear range is 5～100 μg/mL, the correlation coefficient is 0.9986 , the average recovery is 76.2%, the RSD is 3.07%.
出处
《化学分析计量》
CAS
2004年第2期37-38,共2页
Chemical Analysis And Meterage
