Mo-Si-B三元系复合材料的制备及室温断裂韧性

Preparation and Room-Temperature Fracture Toughness of Mo-Si-B Ternary System Composites

通过Mo,Si,B三种单质粉末原位合成热压的方法制备了成分为Mo-12Si-8.5B和Mo-28Si-8.5B的Mo-Si-B三元系复合材料.利用金相显微镜、金相偏光镜、X射线衍射技术、扫描电镜等对制备材料的组织进行了分析,研究了退火工艺对其组织的影响,测量了其室温断裂韧性,并对复合材料的增韧机制进行了初步的探讨.

The alloys containing Mo-12Si-8.5B and Mo-28Si-8.5B respectively were prepared by the in-situ synthesis reaction of the elemental powders of Mo, Si and B by hot-pressing. The microstructures and the annealing processing were investigated by optical microscopy, polariscopy, scanning election microscopy (SEM), and X-ray diSractometry (XRD). The fracture toughness of the alloys at room temperature were determined to be 7.7 and 4.1 MPa·m1/2 respectively. The mechanism for toughening at ambient temperature was discussed.