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阳离子光引发剂芳茂铁六氟磷酸盐的制备 被引量：5

Synthesis of Cationic Photoinitiator [CpFeArene]PF_6
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摘要 以二茂铁为原料制备了3种阳离子光引发剂芳茂铁六氟磷酸盐.考察了反应温度、反应时间和催化剂用量等因素对反应的影响.对产物进行了IR和UV光谱分析. Three kinds of cationic photoinitiator arene-cyclopentadienyl iron hexaflourophosphate salts were prepared with ferrocene.The effect of reactive conditions including reactive temperature,reactive time and the ratio of catalyst to ferrocene were studied.The structure of arene-cyclopentadienyl iron hexaflourophosphate salts were identified by IR and UV spectrum analysis.
作者 刘安昌 莫健华 黄树槐
机构地区 华中科技大学材料工程学院 武汉化工学院化工与制药学院
出处 《感光科学与光化学》 CAS CSCD 北大核心 2004年第3期234-237,共4页 Photographic Science and Photochemistry
关键词 芳茂铁六氟磷酸盐 阳离子光引发剂 cationic photoinitiator arene-cyclopentadienyl iron hexaflourophosphate salt
分类号 TQ572 [化学工程—精细化工]
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参考文献6

  • 1Richard A Brown, Andrew Houlton, Steven D Howe, Roger M G Roberts, Jack Silver. Studies of the bonding in iron (Ⅱ) cyclopentadienyl and arene sandwich compounds part 4 A survey of the effect of methyl substitution on the bonding in same iron sandwich com
  • 2Crivello J V, Lam J H W. Dye-sensitized photoinitiated cationic polymerization[J]. J. Polymn. Sci., Part A, 1978,16,2441-2451.
  • 3Hans Z, Kurt M. Imaging with cationic organometallic photoinitiators [J]. Am. Chem. Soc. Div. Polym. Chem.,1985,26 (2): 347-348.
  • 4Timmons. Cyclopentadienyl iron complex salt, process for preparing the same and photopolymerizable composition containing the same[P]. US Patent ,5 354 784.
  • 5Vincent Desobry, Marly, Hans O Doggweiler, Mohlin. Process for the preparation of organometallic compounds[P].US Patent ,4 992 572.
  • 6王涛,杜洪光,黄毓礼.芳茂铁四氟硼酸盐的制备[J].北京化工大学学报（自然科学版）,2003,30(1):83-85. 被引量：3

二级参考文献6

  • 1[1]Lohse F, Zweifel H. Recent advances in cationic photopolymerization of epoxides[J]. Adv in polym Sci, 1986,78:69-76
  • 2[2]Hans Z, Kurt M. Imaging with cationic organometallic photoinitiators[J]. Am Chem Soc: Div Polym Chem,1985,26(2):347-348
  • 3[3]Timmons. Cyclopentadienyliron complex salt, process for preparing the same and photopolymerizable composition containing the same[P]. USP 5354784. 1994-10-11
  • 4[4]William H, Morrison, Ellen Y, et al. Reaction of ferrocene with polyaromatic molecules[J]. J Am Chem Soc, 1974,29:237-242
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  • 6[6]Astruc D, Dabard R. Organo-iron complexes of aromatic compounds[J]. Tetrahedron, 1983,39(24):4027-4095

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感光科学与光化学
2004年 第3期

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