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部分甲基化β-环糊精混合物的制备及表征 被引量:1

Preparation and Characteristics of Partially Methylated β-Cyclodextrin Mixture
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摘要 采用溶剂沉淀法制备了混合甲基化b-环糊精,并利用IR、X-衍射、透射电镜和同步热分析法对产物的结构进行了表征。制备收率89%左右,操作简便,反应时间短。 Partially methylated b-cyclodextrin was preparated by solvent-precipitation of b-cyclodextrin with(CH3)2SO4 in the presence of Ba2+ in a yield of 89%.
出处 《中国医药工业杂志》 CAS CSCD 北大核心 2004年第5期289-291,共3页 Chinese Journal of Pharmaceuticals
基金 云南省教育厅青年基金资助项目(200142042) 云南省教育厅面上基金资助项目(02ZY175)
关键词 部分甲基化β-环糊精 制备 表征 partially methylated b-cyclodextrin mixture prepaaration characteristics
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  • 1高萍萍,陆光裕.部分甲基化β-环糊精的制备[J].中国医药工业杂志,1995,26(3):105-106. 被引量:9
  • 2戴荣继.特殊选择性气相色谱手性固定相的合成及性能研究.北京理工大学学位论文[M].-,1994.36.
  • 3Henderik W. Frijlink,Anko C. Eissens,Nanco R. Hefting,Klaas Poelstra,Coenraad F. Lerk,Dirk K. F. Meijer. The Effect of Parenterally Administered Cyclodextrins on Cholesterol Levels in the Rat[J] 1991,Pharmaceutical Research(1):9~16

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  • 1冷巍,丁婉萍,唐星.雌二醇甲基化-β-环糊精包合物鼻黏膜吸收动力学研究[J].沈阳药科大学学报,2005,22(3):171-175. 被引量:3
  • 2刘彦生,王宪利.姜黄素甲基化-β-环糊精包合物制备工艺研究[J].武警医学,2007,18(5):337-339. 被引量:12
  • 3李文德,周俊侠,张力田.环糊精的改性研究及进展[J].中国粮油学报,1997,12(1):29-31. 被引量:6
  • 4Lehn J M. Supramolecular chemistry - scope and perspectives molecules, superm - olecules, and molecular devices (Nobel Lecture) [J]. Angew Chem Int Edit, 1988, 27:89 -112.
  • 5张衡益,刘育,李莉.纳米超分子化学:从合成受体到功能组装体[M].北京:化学工业出版社,2004.
  • 6Fenyvesi E, Csabal K. Cyclodextrin N 2006, 20 (11): 301 - 303.
  • 7Romain Jacquet, Patrick Favetta, Claire Elfakir, Michel Lafosse. Characterization of a new methylated/3 - cyclodextrin with a low degree of substitution by matrix - assisted laser desorption/ionization mass spectrometry and liquid chromatography using evaporative light scattering detection [J]. Journal of Chromatography A, 2005, 1083 : 106 - 112.
  • 8Arno Hazekamp, Rob Verpoorte. Structure elucidation of the tetrahydrocannabinol complex with randomly methylated β- cyclodextrin [J]. European Journal of Pharmaceutical Sciences, 2006, 29 : 340 - 347.
  • 9Francois - Xavier Legrand, Mathieu Sauthier, Christophe Flahaut, et al. Aqueous hydroformylation reaction mediated by randomly methylated β - cyclodextrin : How substitution degree influences catalytic activity and selectivity [ J]. Journal of Molecular Catalysis A : Chemical, 2009, 303 : 72 - 77.
  • 10Francois - Xavier Legrand, Frederic "Hapiot, Sebastien Tilloy, et al. Aqueous rhodium- catalyzed hydroformylation of 1 -decene in the presence of randomly methylated β - cyclodextrin and 1,3,5 - triaza - 7 - phosphaadamantane derivatives [ J]. Applied Catalysis A : General, 2009, 362 : 62 - 68.

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