摘要
在冰醋酸中,2,3-二氨基萘通过重氮化反应合成了2,3-二碘萘. 当用稀硫酸作反应介质时,重氮化反应的产物是2,3-萘三唑. 详细的分析了冰醋酸在重氮化反应中的溶剂效应.
diiodonaphthalene was synthesized by Sandmeyer reaction in anhydrous acetic acid. When the solvent was replaced by dilute sulfuric acid, 2,3-naphtho-triazole was obtained. The solvent effect of anhydrous acetic acid was described in detail.
出处
《大连民族学院学报》
CAS
2004年第3期4-5,共2页
Journal of Dalian Nationalities University