烷基取代膦酸二甲酯的合成与表征

Synthesis and Characterization of Alkyl Substituted Dimethyl Phosphonates

以溴戊烷、溴己烷、1,2-二溴乙烷和亚磷酸三甲酯为原料,分别合成了戊基、己基、溴乙基取代的三种膦酸二甲酯化合物.并报道了所合成的化合物的红外光谱、核磁共振氢谱及核磁共振碳谱的数据.

In this paper, three alkyl substituted dimethyl phosphonates have been synthesized by trimethyl phosphite with 1-Bromopentane, 1-Bromohexane and 1,2-Dibromoethane. IR, 1H-NMR and 13 C-NMR data of these compounds have been reported.