摘要
用碳酸钠控制pH ,四丁基溴化胺为相转移催化剂 ,将氮芥苯甲酸与溴代乙酰糖 (溴代乙酰葡萄糖、溴代乙酰半乳糖、溴代乙酰乳糖 )反应 ,合成了 3个氮芥苯甲酸糖酯 ,经IR、1
Three new glucosyl esters of p [N,N bis(2 chloroethyl)amino]benzoic acid were synthesized by the reaction of p [N,N bis(2 chloroethyl)amino]benzoic acid with O acetylglucopyranosyl bromide or O acetylgallactopyranosyl bromide, O acetyllactopyranosyl bromide in the presence of Bu 4NBr and Na 2CO 3.Their structures were identified by elemental analysis,IR,and 1HNMR .
出处
《化学试剂》
CAS
CSCD
北大核心
2004年第3期183-184,共2页
Chemical Reagents
关键词
氮芥苯甲酸
溴代乙酰基糖
相转移催化
p-[N,N-bis(2-chloroethyl)amino]benzoic acid
O-acetyllactopyranosyl bromide