摘要
用液-液、固-液相转移催化法及高温催化法合成了DANP。详细探讨了液-液相转移催化法合成DANP时催化剂种类与用量、溶剂种类与用量以及反应物浓度等因素对DANP产率的影响。用元素分析、质谱、红外光谱、氢核磁共振话对DANP的结构进行了验证。
DANP is synthesized through three different methods with the highest yeild of 67.2%.The main factors influencing the synthesizing process of liquid-liquid catalysis are discussed in detail. The molecule structure of DANP is verified through EMA, IR, NMR, and MS.
出处
《玻璃钢/复合材料》
CAS
CSCD
1993年第6期25-29,共5页
Fiber Reinforced Plastics/Composites