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Mesolamellar composite of TiN and CTAB using fluoride ion bridge: synthesis, mechanism &characterization

Mesolamellar composite of TiN and CTAB using fluoride ion bridge: synthesis, mechanism &characterization
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摘要 In an attempt to synthesize hexagonal mesopo- rous titanium nitride, a mesolamellar composite based on titanium nitride and cetyltrimethylam- monium bromide (CTAB) is obtained by the sol-gel route involving templating at 80oC. The mechanism underlying the above synthesis is discussed for the first time in the literature and till date there are no reports on the synthesis of mesoporous nitrides. The above mesolamellar composite is found to form an oxide of titania (anatase) upon heat treatment at 335oC for 1h. In an attempt to synthesize hexagonal mesopo- rous titanium nitride, a mesolamellar composite based on titanium nitride and cetyltrimethylam- monium bromide (CTAB) is obtained by the sol-gel route involving templating at 80oC. The mechanism underlying the above synthesis is discussed for the first time in the literature and till date there are no reports on the synthesis of mesoporous nitrides. The above mesolamellar composite is found to form an oxide of titania (anatase) upon heat treatment at 335oC for 1h.
机构地区 不详
出处 《Natural Science》 2010年第5期464-468,共5页 自然科学期刊(英文)
关键词 Mesolamellar TEMPLATING SOL-GEL Method XRD FT-IR SEM Mesolamellar Templating Sol-Gel Method XRD FT-IR SEM
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