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Growth and Characterization of Dichloro Tris(Triphenyl Phosphine Oxide)Cadmium(II) —Second Harmonic Generation from a Centrosymmetric Crystal

Growth and Characterization of Dichloro Tris(Triphenyl Phosphine Oxide)Cadmium(II) —Second Harmonic Generation from a Centrosymmetric Crystal
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摘要 The title compound dichloro tris(triphenyl phosphine oxide)cadmium(II) were grown by slow cooling method from aqueous solution. The title compound was synthesized and purified by repeated crystallization process. Grown crystals were characterized by X-ray diffraction and FTIR analysis. The range of optical transmission was determined by recording UV-Vis-NIR spectrum. Thermal properties were investigated by DTA and TGA analyses. Its mechanical hardness was estimated by Vickers microhardness method. The title compound dichloro tris(triphenyl phosphine oxide)cadmium(II) were grown by slow cooling method from aqueous solution. The title compound was synthesized and purified by repeated crystallization process. Grown crystals were characterized by X-ray diffraction and FTIR analysis. The range of optical transmission was determined by recording UV-Vis-NIR spectrum. Thermal properties were investigated by DTA and TGA analyses. Its mechanical hardness was estimated by Vickers microhardness method.
出处 《Journal of Minerals and Materials Characterization and Engineering》 2013年第1期20-23,共4页 矿物质和材料特性和工程(英文)
关键词 CRYSTAL GROWTH Single CRYSTAL X-Ray Diffraction ULTRAVIOLET Spectra Nonlinear Optical Crystals Crystal Growth Single Crystal X-Ray Diffraction Ultraviolet Spectra Nonlinear Optical Crystals
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