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The Synthesis of Solvent-Free TiO<sub>2</sub>Nanofluids through Surface Modification 被引量:1

The Synthesis of Solvent-Free TiO<sub>2</sub>Nanofluids through Surface Modification
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摘要 TiO2 nanoparticles with surface hydroxyl groups are treated by trimethoxysilane (CH3O)3Si(CH2)3O(CH2CH2O)6-9CH3 and a inorganic core/organic shell hybridmaterials, which shows itself a yellow viscous fluid, is obtained. We call it solvent-free TiO2 nanofliuds. Transmission electron microscopy (TEM), Fourier transform infrared spectrum (FTIR), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and rheometer are adopted to characterize the product. As a result, the content of TiO2 nanoparticles in the nanofliuds is about 5.5wt%, the functionalized TiO2 nanoparticles possess better dispersion, very low viscosity and an obvious liquid-like behavior at room temperature in absence of solvent. TiO2 nanoparticles with surface hydroxyl groups are treated by trimethoxysilane (CH3O)3Si(CH2)3O(CH2CH2O)6-9CH3 and a inorganic core/organic shell hybridmaterials, which shows itself a yellow viscous fluid, is obtained. We call it solvent-free TiO2 nanofliuds. Transmission electron microscopy (TEM), Fourier transform infrared spectrum (FTIR), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and rheometer are adopted to characterize the product. As a result, the content of TiO2 nanoparticles in the nanofliuds is about 5.5wt%, the functionalized TiO2 nanoparticles possess better dispersion, very low viscosity and an obvious liquid-like behavior at room temperature in absence of solvent.
出处 《Soft Nanoscience Letters》 2011年第2期46-50,共5页 软纳米科学报(英文)
关键词 SOLVENT-FREE Nanofulids TiO2 NANOPARTICLES Liquid-Like Behave Solvent-Free Nanofulids TiO2 Nanoparticles Liquid-Like Behave
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