Powder metallurgy Ti-45Al-10 Nb alloys was successfully fabricated by reactive sintering of milled powders at 1350 °C for 2 h in vacuum. The microstructure, in particular, constituent phases, grain size, precipit...Powder metallurgy Ti-45Al-10 Nb alloys was successfully fabricated by reactive sintering of milled powders at 1350 °C for 2 h in vacuum. The microstructure, in particular, constituent phases, grain size, precipitates of the product was investigated in detail. The results indicate that a double phase γ+α2 microstructure containing Ti2 Al C precipitate is obtained under the sintering condition, and the alloy exhibits a fine and homogenous microstructure compared with traditional Ti Al base. In fine grain structure, the average grain sizes for the γ and α2 phases are(2.3±0.05) and(5.6±0.05) μm, respectively. Additionally, numerous dislocations are observed in the alloy, and the dislocation density in γ phase is significantly higher than that in α2 phase. The formation mechanisms of the dislocation in the present alloy were also discussed in detail.展开更多
基金supported by the Key Laboratory of Micro-systems and Micro-structures Manufacturing of Ministry of Education,Harbin Institute of Technology,China(No.2020KM005)the Natural Science Foundation of Heilongjiang Province,China(No.YQ2020E030)。
文摘Powder metallurgy Ti-45Al-10 Nb alloys was successfully fabricated by reactive sintering of milled powders at 1350 °C for 2 h in vacuum. The microstructure, in particular, constituent phases, grain size, precipitates of the product was investigated in detail. The results indicate that a double phase γ+α2 microstructure containing Ti2 Al C precipitate is obtained under the sintering condition, and the alloy exhibits a fine and homogenous microstructure compared with traditional Ti Al base. In fine grain structure, the average grain sizes for the γ and α2 phases are(2.3±0.05) and(5.6±0.05) μm, respectively. Additionally, numerous dislocations are observed in the alloy, and the dislocation density in γ phase is significantly higher than that in α2 phase. The formation mechanisms of the dislocation in the present alloy were also discussed in detail.