The effects of the solid solution conditions on the microstructure and tensile properties of Al?Zn?Mg?Cu aluminum alloy were investigated by in-situ resistivity measurement, optical microscopy (OM), scanning electron ...The effects of the solid solution conditions on the microstructure and tensile properties of Al?Zn?Mg?Cu aluminum alloy were investigated by in-situ resistivity measurement, optical microscopy (OM), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and tensile test. A radial basis function artificial neural network (RBF-ANN) model was developed for the analysis and prediction of the electrical resistivity of the tested alloy during the solid solution process. The results show that the model is capable of predicting the electrical resistivity with remarkable success. The correlation coefficient between the predicted results and experimental data is 0.9958 and the relative error is 0.33%. The predicted data were adopted to construct a novel physical picture which was defined as “solution resistivity map”. As revealed by the map, the optimum domain for the solid solution of the tested alloy is in the temperature range of 465?475 °C and solution time range of 50?60 min. In this domain, the solution of second particles and the recrystallization phenomenon will reach equilibrium.展开更多
The microstructure evolution and properties of an Al-Zn-Mg-Cu alloy were investigated under different non-linear cooling processes from the solution temperature, combined with in-situ electrical resistivity measuremen...The microstructure evolution and properties of an Al-Zn-Mg-Cu alloy were investigated under different non-linear cooling processes from the solution temperature, combined with in-situ electrical resistivity measurements, selected area diffraction patterns （SADPs）, transmission electron microscopy （TEM）, and tensile tests. The relative resistivity was calculated to characterize the phase transformation of the experimental alloy during different cooling processes. The results show that at high temperatures, the microstructure evolutions change from the directional diffusion of Zn and Mg atoms to the precipitation of S phase, depending on the cooling rate. At medium temperatures, q phase nucleates on A13Zr dispersoids and grain boundaries under fast cooling conditions, while S phase precipitates under the slow cooling conditions. The strength and ductility of the aged alloy suffer a significant deterioration due to the heterogeneous precipitation in medium temperature range. At low temperatures, homogeneously nucleated GP zone, η′ and η phases precipitate.展开更多
The effect of Hf on the grain refinement of as-cast aluminum was investigated using optical microscopy, electron microscopy and X-ray diffraction. The result shows that the grain size of studied alloy decreases effect...The effect of Hf on the grain refinement of as-cast aluminum was investigated using optical microscopy, electron microscopy and X-ray diffraction. The result shows that the grain size of studied alloy decreases effectively with the addition of Hf,Hf can react with Al to form Al3Hf particles during the solidification, the primary Al3Hf particles are highly potent nucleants for Al and the nanoscale coherent Al3Hf particles can inhibit the grain growth by pinning effect. The grain refinement mechanism of studied alloys was verified by the solute theory and the crystallography study, and it can be divided into two distinct types: At low Hf contents, there are no primary Al3Hf phases to form, the acquired grain refinement is primarily attributed to the constitutional undercooling induced by the Hf solute. At medium and high Hf contents, both Hf solute and Al3Hf particles contribute to the refinement.展开更多
基金Project(51344004)supported by the National Natural Science Foundation of China
文摘The effects of the solid solution conditions on the microstructure and tensile properties of Al?Zn?Mg?Cu aluminum alloy were investigated by in-situ resistivity measurement, optical microscopy (OM), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and tensile test. A radial basis function artificial neural network (RBF-ANN) model was developed for the analysis and prediction of the electrical resistivity of the tested alloy during the solid solution process. The results show that the model is capable of predicting the electrical resistivity with remarkable success. The correlation coefficient between the predicted results and experimental data is 0.9958 and the relative error is 0.33%. The predicted data were adopted to construct a novel physical picture which was defined as “solution resistivity map”. As revealed by the map, the optimum domain for the solid solution of the tested alloy is in the temperature range of 465?475 °C and solution time range of 50?60 min. In this domain, the solution of second particles and the recrystallization phenomenon will reach equilibrium.
基金Project(2014GK2013)supported by the Science and Technology Program of Hunan Province,China
文摘The microstructure evolution and properties of an Al-Zn-Mg-Cu alloy were investigated under different non-linear cooling processes from the solution temperature, combined with in-situ electrical resistivity measurements, selected area diffraction patterns （SADPs）, transmission electron microscopy （TEM）, and tensile tests. The relative resistivity was calculated to characterize the phase transformation of the experimental alloy during different cooling processes. The results show that at high temperatures, the microstructure evolutions change from the directional diffusion of Zn and Mg atoms to the precipitation of S phase, depending on the cooling rate. At medium temperatures, q phase nucleates on A13Zr dispersoids and grain boundaries under fast cooling conditions, while S phase precipitates under the slow cooling conditions. The strength and ductility of the aged alloy suffer a significant deterioration due to the heterogeneous precipitation in medium temperature range. At low temperatures, homogeneously nucleated GP zone, η′ and η phases precipitate.
基金Project(SGRI-WD-71-13-001) supported by the Scientific and Technological Project of State Grid Corporation of China
文摘The effect of Hf on the grain refinement of as-cast aluminum was investigated using optical microscopy, electron microscopy and X-ray diffraction. The result shows that the grain size of studied alloy decreases effectively with the addition of Hf,Hf can react with Al to form Al3Hf particles during the solidification, the primary Al3Hf particles are highly potent nucleants for Al and the nanoscale coherent Al3Hf particles can inhibit the grain growth by pinning effect. The grain refinement mechanism of studied alloys was verified by the solute theory and the crystallography study, and it can be divided into two distinct types: At low Hf contents, there are no primary Al3Hf phases to form, the acquired grain refinement is primarily attributed to the constitutional undercooling induced by the Hf solute. At medium and high Hf contents, both Hf solute and Al3Hf particles contribute to the refinement.
