Hierarchical europium oxalate Eu2(C2O4)3.10H2O micro-particles were synthesized through a simple precipitation method at room temperature in present of trisodium citrate. The products were characterized by X-ray dif...Hierarchical europium oxalate Eu2(C2O4)3.10H2O micro-particles were synthesized through a simple precipitation method at room temperature in present of trisodium citrate. The products were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, field-emission scanning electron microscopy, and photoluminescence. The possible formation mechanism of the hierarchical europium oxalate Eu2(C2O4)3.10H2O micro-particles was discussed.展开更多
Flower-like NaY(MoO4)2 particles were synthesized through a microwave-assisted hydrother- mal process followed by a subsequent calcination process. The products were characterized by X-ray diffraction, X-ray photoel...Flower-like NaY(MoO4)2 particles were synthesized through a microwave-assisted hydrother- mal process followed by a subsequent calcination process. The products were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, field-emission scanning electron mi- croscopy. The possible formation mechanism of the flower-like NaY(MoO4)2 precursor was proposed. The NaY(MoO4)2:Eu3+ phosphors were also prepared and their luminescence properties showed the NaY(MoO4)2:Eu^3+ materials with the emission peak at 612 nm had potential application as a red phosphor for white light-emitting diodes. Furthermore, the microwave-assisted hydrothermal process followed by a subsequent calcination process could be extended to prepare the other lanthanide molybdates with the flower-like morphology.展开更多
文摘Hierarchical europium oxalate Eu2(C2O4)3.10H2O micro-particles were synthesized through a simple precipitation method at room temperature in present of trisodium citrate. The products were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, field-emission scanning electron microscopy, and photoluminescence. The possible formation mechanism of the hierarchical europium oxalate Eu2(C2O4)3.10H2O micro-particles was discussed.
文摘Flower-like NaY(MoO4)2 particles were synthesized through a microwave-assisted hydrother- mal process followed by a subsequent calcination process. The products were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, field-emission scanning electron mi- croscopy. The possible formation mechanism of the flower-like NaY(MoO4)2 precursor was proposed. The NaY(MoO4)2:Eu3+ phosphors were also prepared and their luminescence properties showed the NaY(MoO4)2:Eu^3+ materials with the emission peak at 612 nm had potential application as a red phosphor for white light-emitting diodes. Furthermore, the microwave-assisted hydrothermal process followed by a subsequent calcination process could be extended to prepare the other lanthanide molybdates with the flower-like morphology.
基金National Key R&D Program of China(2017YFF0108402,2016YFC1400602)National Natural Science Foundation(61805255,61378041)+2 种基金Anhui Natural Science Foundation(1808085MF208)Anhui Key Research and Development Plan Project(1804a0802192)Anhui Province Science and Technology Major Project(17030801033)
基金supported by National Natural Science Foundation(61805255,61378041)National Key R&D Program of China(2017YFF0108402,2016YFC1400602)+2 种基金Anhui Natural Science Foundation(1808085MF208)Anhui Key Research and Development Plan Project(1804a0802192)Anhui Province Science and Technology Major Project(17030801033)。