A continuous melt suspension crystallization process has been presented for the purification of the phosphoric acid in this study, which is performed in the cascade of a mixed suspension mixed product removal (MSMPR) ...A continuous melt suspension crystallization process has been presented for the purification of the phosphoric acid in this study, which is performed in the cascade of a mixed suspension mixed product removal (MSMPR) crystallizer and a gravity wash column for the subsequent solid-liquid separation. Dynamic behavior in the crystallizer and role of reflux ration on the purification efficiency of column are studied in detail. A reasonable steady state with respect to the liquid phase is achieved after 2 to 3 hrs, which is followed by a solid-phase steady state in terms of the slurry density after 4 hrs. Reflux ratio is the effective parameter for separation and purification by the crystallization equipment from the influences of reflux ratio on the purity of product, the number of theoretical plates and the stability of the operations.展开更多
Although the uniformity of diamond discrete global grid is essential for calculations and searches,geometric deformations increase with the level of divisions.The Good child Criteria provides a basis for evaluating th...Although the uniformity of diamond discrete global grid is essential for calculations and searches,geometric deformations increase with the level of divisions.The Good child Criteria provides a basis for evaluating the quality of the global grid.However,some indicators in the criteria are redundant and contradictory,and the existing indicator system has limitations.Directly using the indicator system may render the evaluation of the diamond grid unreliable.In this study,we summarized the evaluation indicators for grid quality basedon the Good child Criteria,calculated the correlations between these indicators using different diamond grid systems,and constructed reliable evaluation systems based on similarities and differences.The selected grid systems are classified into two groups:non-equal-area and equal-area grids.Their quality evaluation systems are composed of Size-Shape-Topology Factor and Geometry-Topology Factor,respectively.The proposed quality evaluation systems utilize a minimal number of indicators selected from each factor to provide a comprehensive description of the diamondgrid’s characteristics.This approach simplifies the complexity of the evaluations while improving their reliability and credibility.展开更多
文摘A continuous melt suspension crystallization process has been presented for the purification of the phosphoric acid in this study, which is performed in the cascade of a mixed suspension mixed product removal (MSMPR) crystallizer and a gravity wash column for the subsequent solid-liquid separation. Dynamic behavior in the crystallizer and role of reflux ration on the purification efficiency of column are studied in detail. A reasonable steady state with respect to the liquid phase is achieved after 2 to 3 hrs, which is followed by a solid-phase steady state in terms of the slurry density after 4 hrs. Reflux ratio is the effective parameter for separation and purification by the crystallization equipment from the influences of reflux ratio on the purity of product, the number of theoretical plates and the stability of the operations.
基金funded by the Yunnan Provincial Education Department Scientific Research Fund Project[grant number 2023J0717]the Applied Basic Research Foundation of Yunnan Province[grant number 2019FB067].
文摘Although the uniformity of diamond discrete global grid is essential for calculations and searches,geometric deformations increase with the level of divisions.The Good child Criteria provides a basis for evaluating the quality of the global grid.However,some indicators in the criteria are redundant and contradictory,and the existing indicator system has limitations.Directly using the indicator system may render the evaluation of the diamond grid unreliable.In this study,we summarized the evaluation indicators for grid quality basedon the Good child Criteria,calculated the correlations between these indicators using different diamond grid systems,and constructed reliable evaluation systems based on similarities and differences.The selected grid systems are classified into two groups:non-equal-area and equal-area grids.Their quality evaluation systems are composed of Size-Shape-Topology Factor and Geometry-Topology Factor,respectively.The proposed quality evaluation systems utilize a minimal number of indicators selected from each factor to provide a comprehensive description of the diamondgrid’s characteristics.This approach simplifies the complexity of the evaluations while improving their reliability and credibility.
