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气相色谱法测定6种不同基质化妆品中水杨酸甲酯含量 被引量:1
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作者 汪亚菁 贾伯阳 +1 位作者 邬国庆 邸铮 《日用化学工业(中英文)》 CAS 北大核心 2023年第3期355-360,共6页
建立了气相色谱法(GC)测定6种基质化妆品中水杨酸甲酯的方法,并采用气相色谱-串联质谱法(GC-MS)对目标物进行定性确证。蜡基样品经乙酸乙酯-无水乙醇提取,其他基质样品经无水乙醇提取后,采用气相色谱-氢火焰离子化检测器进行测定。GC-M... 建立了气相色谱法(GC)测定6种基质化妆品中水杨酸甲酯的方法,并采用气相色谱-串联质谱法(GC-MS)对目标物进行定性确证。蜡基样品经乙酸乙酯-无水乙醇提取,其他基质样品经无水乙醇提取后,采用气相色谱-氢火焰离子化检测器进行测定。GC-MS采用全扫(SCAN)与选择离子监测(SIM)方式对结果进行确认。水杨酸甲酯质量浓度在5~500 mg/L范围内与其峰面积呈良好的线性关系(r=0.999 9);6种基质在高、中、低三个浓度加标的平均回收率为96.9%~108.2%,相对标准偏差(RSD)均≤2.9%(n=6);方法检出限为4μg/g,定量限为100μg/g;方法用于不同基质样品的分析,其中1批润唇膏检出水杨酸甲酯含量为0.083%,超出了欧盟对此类产品的限值要求。该方法快速、准确,适用于不同基质化妆品中水杨酸甲酯的定性定量分析,为化妆品中水杨酸甲酯的测定与筛查提供了技术支持。 展开更多
关键词 水杨酸甲酯 气相色谱法 气相色谱-串联质谱法 化妆品
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Simulation of the effect of a magnetically insulated anode on a low-power cylindrical Hall thruster 被引量:1
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作者 Yongjie DING Hong LI +7 位作者 boyang jia Peng LI Liqiu WEI Yu XU Wuji PENG Hezhi SUN Yong CAO Daren YU 《Plasma Science and Technology》 SCIE EI CAS CSCD 2018年第3期156-162,共7页
The intersection point of the characteristic magnetic field line(CMFL) crossing the anode boundary with the discharge channel wall, and its influence on thruster performance and the energy and flux of ions bombardin... The intersection point of the characteristic magnetic field line(CMFL) crossing the anode boundary with the discharge channel wall, and its influence on thruster performance and the energy and flux of ions bombarding the channel wall, have been studied numerically. The simulation results demonstrate that with the increase in distance from the crossover point of the CMFL with the channel wall to the bottom of the thruster channel, the ionization rate in the discharge channel gradually increases; meanwhile, the ion energy and ion current density bombarding the channel wall decreases. When the point of the CMFL with the channel wall is at the channel outlet, the thrust, specific impulse, and efficiency are at a maximum, while the ion energy and ion current density bombarding the channel wall are at a minimum. Therefore, to improve the performance and lifetime of the thruster, it is important to control the point of intersection of the CMFL with the channel wall. 展开更多
关键词 magnetically insulated anode cylindrical Hall thruster PERFORMANCE
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