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三组分反应合成5-(4-甲基苯基)-3-三氟甲基-1H-吡唑的综合实验设计
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作者 彭荣斌 周尚 +2 位作者 汪子阳 林东恩 竺传乐 《大学化学》 CAS 2023年第8期248-258,共11页
通过科研反哺教学,本实验将“多组分反应”和“含氟有机化合物”融入到本科实验教学中,通过三组分反应合成了5-(4-甲基苯基)-3-三氟甲基-1H-吡唑。该实验条件温和,操作简单,分离产率高,重现性好,安全性高。该综合实验能帮助学生理解步... 通过科研反哺教学,本实验将“多组分反应”和“含氟有机化合物”融入到本科实验教学中,通过三组分反应合成了5-(4-甲基苯基)-3-三氟甲基-1H-吡唑。该实验条件温和,操作简单,分离产率高,重现性好,安全性高。该综合实验能帮助学生理解步骤经济性合成的概念,建立绿色化学的理念,是适合引入有机实验教学课程的新课题。 展开更多
关键词 有机氟化学 多组分反应 3-三氟甲基-1H-吡唑 含氟砌块
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Smoke Hazard Assessment Model Based on Fire Dynamics Simulator and FED Model 被引量:2
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作者 Nianfeng Li shang zhou +1 位作者 Zhiguo Xiao Yifei Zhao 《Journal of Computer and Communications》 2020年第9期81-93,共13页
Smoke is the main cause of fire death. In order to minimize the potential danger of smoke hazard, a rational VR based fire training simulator should fully consider all aspects of smoke hazard. In the simulator, the vi... Smoke is the main cause of fire death. In order to minimize the potential danger of smoke hazard, a rational VR based fire training simulator should fully consider all aspects of smoke hazard. In the simulator, the visualization of data based on FDS (Fire Dynamics Simulator) and FED fire dynamic data and volume rendering is further optimized, which can be effectively and quickly applied to virtual fire protection. In addition, a comprehensive smoke hazard assessment model based on FED and FED is established to assess the IHD value of different paths, which represents the safety of different paths, and can be used for evacuation or rescue in virtual training. Taking the case of campus fire drill as an experiment, the research shows the accuracy and effectiveness of smoke assessment based on FDS and FED model. The road force with the highest safety can be selected through the comprehensive model. So the assessment model is proved to be valuable. 展开更多
关键词 Smoke Hazard Smoke Visualization Integrated Smoke Assessment Model FDS FED
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Research on Key Technologies of Hand Function Rehabilitation Training Evaluation System Based on Leap Motion 被引量:1
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作者 Zhiguo Xiao Yifei Zhao +2 位作者 Nianfeng Li shang zhou Hu Xu 《Journal of Computer and Communications》 2021年第1期19-35,共17页
This paper proposes an immersive training system for patients with hand dysfunction who can perform rehabilitation training independently. The system uses Leap Motion binocular vision sensors to collect human hand inf... This paper proposes an immersive training system for patients with hand dysfunction who can perform rehabilitation training independently. The system uses Leap Motion binocular vision sensors to collect human hand information, and uses the improved PCA<sub><img src="Edit_d6662636-9073-4fbd-855f-9a36e871d5a4.png" width="10" height="15" alt="" /></sub> (Principal Component Analysis) to perform data fusion on the real-time data collected by the sensor to obtain more hands with fewer principal components, and improve the stability and accuracy of the data. Immediately, the use of improved SVM<sub><img src="Edit_10c78725-e09e-4dcf-ae05-e21205df4acc.png" width="10" height="15" alt="" /></sub> (Support Vector Machine) and KNN<sub><img src="Edit_0ee97f55-2773-4b48-93b3-93f61aa25577.png" width="10" height="15" alt="" /></sub> (K-Nearest Neighbor Algorithm) for gesture recognition and classification is proposed to enable patients to perform rehabilitation training more effectively. Finally, the effective evaluation results of the rehabilitation effect of patients by the idea of AHP<sub><img src="Edit_70dd1964-28be-4137-afa5-9a184704f08e.png" width="10" height="15" alt="" /></sub> (Analytic Hierarchy Process) are taken as necessary reference factors for doctors to follow up treatment. Various experimental results show that the system has achieved the expected results and has a good application prospect. 展开更多
关键词 Leap Motion IMMERSIVE AHP PCA SVM KNN Hand Function Rehabilitation Evaluation System
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5G多维度鼠标
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作者 周文镜 商周 +1 位作者 彭麒锜 王莉 《价值工程》 2020年第7期259-261,共3页
5G多维度鼠标是随着AI发展,基于5G性能进化出的新的输入方式,可以作为第一代5G输入设备。其具有移动与旋转的运动方式及感应、摆动、按键、移动的输入形式,优化的控制电路,智能化的信息传输流程。结合虚拟现实技术,5G多维度鼠标将书写... 5G多维度鼠标是随着AI发展,基于5G性能进化出的新的输入方式,可以作为第一代5G输入设备。其具有移动与旋转的运动方式及感应、摆动、按键、移动的输入形式,优化的控制电路,智能化的信息传输流程。结合虚拟现实技术,5G多维度鼠标将书写人们美好的未来。 展开更多
关键词 5G多维度鼠标 虚拟现实 控制电路 5G输入设备
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La0.9Rb0.1Co1-xFexO3-δ钙钛矿催化剂上NOx辅助碳烟燃烧性能的研究 被引量:4
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作者 车祥 汪炜 +3 位作者 商周 王丽 郭耘 卢冠忠 《稀有金属》 EI CAS CSCD 北大核心 2018年第6期650-656,共7页
通过柠檬酸溶胶凝胶法制备了La0.9Rb0.1Co1-xFexO3-δ(x=0.1~0.8)系列钙钛矿催化剂。通过X射线衍射(XRD)、氢气程序升温还原(H2-TPR)、NOx程序升温脱附(NOx-TPD)及X射线光电子能谱(XPS)考察了Fe含量变化对催化剂结构、NOx辅... 通过柠檬酸溶胶凝胶法制备了La0.9Rb0.1Co1-xFexO3-δ(x=0.1~0.8)系列钙钛矿催化剂。通过X射线衍射(XRD)、氢气程序升温还原(H2-TPR)、NOx程序升温脱附(NOx-TPD)及X射线光电子能谱(XPS)考察了Fe含量变化对催化剂结构、NOx辅助碳烟燃烧反应活性、催化剂氧化还原活性、催化剂表面Fe和Co的化学状态以及NOx储存能力的影响。结果表明:所制备的催化剂均保持钙钛矿结构,Co与Fe的共掺杂改变了B位金属的化学状态,催化剂表面存在Co2+和更高价态的Fe物种。相比纯LaCoO3和LaFeO3,La0.9Rb0.1Co1-xFexO3-δ(x=0.1~0.8)催化剂碳烟燃烧的特征温度T50分别下降约30和70℃,碳烟燃烧的速度也随之加快。同时,在NOx辅助碳烟燃烧过程中,NO氧化所生成的NO2可与碳烟反应生成N2,其中La0.9Rb0.1Co0.6Fe0.4O3-δ催化剂具有最高的NOx消除能力,在381℃时达到36.4%。 展开更多
关键词 钙钛矿 La0.9Rb0.1Co1-xFexO3-δ NOx辅助碳烟燃烧 NOx储存
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Synthesis and photoluminescence of Ca1-xTiO3 :xEu^3+ nanoparticles
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作者 shang zhou Hua Wang +3 位作者 Li Zhong Junqian Zhao Liang Li Guanghai Li 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2018年第6期949-954,共6页
Ca1-xTiO3 :xEu^3+ nanoparticles (NPs) with the size ranging from 27 nm to 135 nm were prepared by means of a chemical co-precipitation method. The structural and optical properties of the NPs were investigated, an... Ca1-xTiO3 :xEu^3+ nanoparticles (NPs) with the size ranging from 27 nm to 135 nm were prepared by means of a chemical co-precipitation method. The structural and optical properties of the NPs were investigated, and the influence of Eu doping content and sintering temperature on the photoluminescence of the Ca1-xTiO3 :xEu^3+ NPs were examined. An obvious red emission band centered at 615 nm were observed under the excitation with 395 nm for the Ca1-xTiO3 :xEu^3+ NPs. X-ray photoelectron spectroscopy analyses suggest that Eu^3+ is incorporated into not only the Ca-site, but also Ti-site of CaTiO3 crystal lattice. Our study shows the promise of the Ca1-xTiO3 :xEu^3+ NPs as a red nanophosphor. 展开更多
关键词 Calcium titanate Nanoparticles Photoluminescence Red phosphor Crystal structure
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