With a series of 1.0 wt%Bi_(2)O_(3)-x wt%CuO(x=0.0,0.2,0.4,0.6,and 0.8)serving as sintering additives,Ni_(0.23)Cu_(0.32)Zn_(0.45)Ee_(2)O_(4)ferrites are successfully synthesized at a low temperature(900℃)by using the...With a series of 1.0 wt%Bi_(2)O_(3)-x wt%CuO(x=0.0,0.2,0.4,0.6,and 0.8)serving as sintering additives,Ni_(0.23)Cu_(0.32)Zn_(0.45)Ee_(2)O_(4)ferrites are successfully synthesized at a low temperature(900℃)by using the solid state reaction method.The effects of the additives on the phase formation,magnetic and dielectric properties as well as the structural and gyromagnetic properties are investigated.The x-ray diffraction(XRD)results indicate that the added Bi_(2)O_(3)-CuO can lower the synthesis temperature significantly without the appearing of the second phase.The scanning electron microscope(SEM)images confirm that Bi_(2)O_(3)is an important factor that determines the sintering behaviors,while CuO affects the grain size and densification.With CuO content x=0.4 or 0.6,the sample shows high saturation magnetization,low coercivity,high real part of magnetic permeability,dielectric permittivity,and small ferromagnetic resonance linewidth(ΔH).The NiCuZn ferrites are a promising new generation of high-performance microwave devices,such as phase shifters and isolators.展开更多
The Ca-Sn co-substituted yttrium iron garnet(YIG)ferrite materials were prepared by the traditional oxide solid-state reaction method,and the influence of forming pressure on the density,morphology and magnetic proper...The Ca-Sn co-substituted yttrium iron garnet(YIG)ferrite materials were prepared by the traditional oxide solid-state reaction method,and the influence of forming pressure on the density,morphology and magnetic properties of YIG ferrite was systematically studied.The results show that the density of YIG ferrite green body increases with the increase of the forming pressure,while the density of its sintered body shows a trend of first increasing and then decreasing.At the same time,the ferromagnetic resonance(FMR)linewidth of YIG sample first decreases and then increases.Meanwhile,the effects of forming pressure on the saturation magnetization,remanence and coercivity of the sample can be ignored.This study proves that the density and FMR linewidth of YIG materials can be controlled by regulating the forming pressure and the best performance is obtained for the sample prepared under a forming pressure of 5 MPa.展开更多
基金Project supported by the National Key Research and Development Program of China(Grant No.2018YFE0115500)the National Natural Science Foundation of China(Grant Nos.52003256 and 51902037)the Natural Science Foundation of Shanxi Province,China(Grant No.201901D211259)。
文摘With a series of 1.0 wt%Bi_(2)O_(3)-x wt%CuO(x=0.0,0.2,0.4,0.6,and 0.8)serving as sintering additives,Ni_(0.23)Cu_(0.32)Zn_(0.45)Ee_(2)O_(4)ferrites are successfully synthesized at a low temperature(900℃)by using the solid state reaction method.The effects of the additives on the phase formation,magnetic and dielectric properties as well as the structural and gyromagnetic properties are investigated.The x-ray diffraction(XRD)results indicate that the added Bi_(2)O_(3)-CuO can lower the synthesis temperature significantly without the appearing of the second phase.The scanning electron microscope(SEM)images confirm that Bi_(2)O_(3)is an important factor that determines the sintering behaviors,while CuO affects the grain size and densification.With CuO content x=0.4 or 0.6,the sample shows high saturation magnetization,low coercivity,high real part of magnetic permeability,dielectric permittivity,and small ferromagnetic resonance linewidth(ΔH).The NiCuZn ferrites are a promising new generation of high-performance microwave devices,such as phase shifters and isolators.
文摘The Ca-Sn co-substituted yttrium iron garnet(YIG)ferrite materials were prepared by the traditional oxide solid-state reaction method,and the influence of forming pressure on the density,morphology and magnetic properties of YIG ferrite was systematically studied.The results show that the density of YIG ferrite green body increases with the increase of the forming pressure,while the density of its sintered body shows a trend of first increasing and then decreasing.At the same time,the ferromagnetic resonance(FMR)linewidth of YIG sample first decreases and then increases.Meanwhile,the effects of forming pressure on the saturation magnetization,remanence and coercivity of the sample can be ignored.This study proves that the density and FMR linewidth of YIG materials can be controlled by regulating the forming pressure and the best performance is obtained for the sample prepared under a forming pressure of 5 MPa.
