FePt granular films were prepared by direct current facing-target magnetron sputtering system onto glass substrates and subsequently in-situ annealed in vacuum. Vibrating sample magnetometer, X-ray diffraction and sca...FePt granular films were prepared by direct current facing-target magnetron sputtering system onto glass substrates and subsequently in-situ annealed in vacuum. Vibrating sample magnetometer, X-ray diffraction and scanning probe microscope were applied to study the magnetic properties, microstructures, morphologies and domain structures of the samples. （FePt）27Ti73 bilayer films were fabricated at various conditions to investigate the effect of Ti on FePt grains. The results show that without Ti matrix layer, FePt films deposited onto the glass substrates are fcc disordered; with addition of Ti matrix layer, FePt/Ti films form a ternary （FePt）27Ti73 alloy possessing fcc and L10 （111） mixed texture. FePt/（FePt）27Ti73 films with perfectly ordered L10（111） structure and unique magnetic properties can be obtained at Ti thickness of 35nm and substrate temperature of 250℃. The maximum coercivity is more than 240kA/m and the squareness ratio is more than 0.9. The obtained results suggest that the granular FePt/（FePt）27Ti73 films can be applicable to ultrahigh-density magnetic recording media.展开更多
A new brush plating process with a soluble anode of nickel was introduced. TDY112 brush plating solution was used on the No.20 carbon steel substrate. It has the higher deposit velocity, better properties and lower co...A new brush plating process with a soluble anode of nickel was introduced. TDY112 brush plating solution was used on the No.20 carbon steel substrate. It has the higher deposit velocity, better properties and lower cost. Scanning electronic microscopy(SEM), optical microscope, microhardness test and wear test were adopted to detect the surface quality and the properties of the coating, such as micrograph, microstructure, micro-hardness wear resistance and adherence between the coating and the substrate. The experimental results showed that the suitable technological parameters to be used, the coatings had better the surface quality, higher hardness and wear resistance.展开更多
As a new technology, Atomil Force Microscopy （AFM） is being used in the research of microscopic structure on coal surface in recent years. By this technology, we can observe the nanoscale pore and crack shape of coa...As a new technology, Atomil Force Microscopy （AFM） is being used in the research of microscopic structure on coal surface in recent years. By this technology, we can observe the nanoscale pore and crack shape of coal surface, and measure some structural parameters. Different metamorphic grades produce different feature of surface microscopic structure of coal. This paper analyzes the surface microscopic structure of different metamorphic grade coal by AFM. The results show that the coal surface microstructure has a trend from rough to smooth with the increasing of metamorphic grade. The low rank coals contain large or medium pores and the high rank coals contain micro pores. The values of surface morphology characteristic parameters （Sq and Sa） nonlinearly decrease with the increasing coal rank. That is, the coal surface becomes smoother during coalification.展开更多
EPD （electrophoretic deposition） technique has been shown as an effective method to produce thin ore thick layers at voltage 5-100 V onto Ni conductive substrate. The aim of this study is to use the EPD method to fa...EPD （electrophoretic deposition） technique has been shown as an effective method to produce thin ore thick layers at voltage 5-100 V onto Ni conductive substrate. The aim of this study is to use the EPD method to fabricate films from suspensions BaTiO3. The effects of the EPD process parameters such as the suspension concentration, deposition time, electrical field strength on the specific EPD deposited weight, morphology particles were used. The surface microstructures of the as-deposited films were investigated by SEM （scanning electron microscopy）. A homogeneous microstructure was obtained at applied electric field of 100 V and I min of deposition time at an electrode distance of 1.0 cm.展开更多
Objective To observe the surface structures of cardiovascular endothelial cells in situ with atomic force microscope （AFM）. Methods Fresh aorta and aortic valve were dissected from 10 healthy male New Zealand white ...Objective To observe the surface structures of cardiovascular endothelial cells in situ with atomic force microscope （AFM）. Methods Fresh aorta and aortic valve were dissected from 10 healthy male New Zealand white rabbits. Before fixed in 1% formaldehyde, the fresh tissues were washed in the buffer phosphate solution. Under general microscope, the fixed aorta or valve was spread on the double side stick tape which had already been stuck on the glass slide. The intima of aorta or the aorta side of valve was towards upside, Then the specimen was dried under 37 degrees centigrade in an attemperator and was washed with pure water. After dried again, the specimen was loaded on the platform ofNanoScope Ⅲa AFM and was scanned in tapping mode with the scanning speed of 0.5 HZ. Results The surface structures of endothelial cell on the fixed and dried tissue could be observed clearly in situ with AFM. aortic endothelial cells were large, branched and arranged sparsely and parallel to the direction of blood flow, whereas endothelial cells on aorta valve surface were small, less branched and arranged intensively and vertical to the direction of blood flow. When the scanning range was dwindled, granular ultra-structures could be observed on the surface of endothelial cells, and, as the scanning range was dwindled further, fissure and convolution could be seen on the surface of granules from aortic endothelial cells. Centre cavity and surrounding swelling volcano-like structure could be seen on the surface of granules from endothelial cells of aortic valve. Conclusions It＇s feasible to observe the surface ultra-structures of cardiovascular endothelial cells in situ with AFM and morphological information provided by AFM might be of clinical value in future histopathological diagnosis（JGeriatr Cardiol2009; 6：178-181）.展开更多
The magnetic domain structures of the 100 oriented Fe 81 Ga 19 polycrystalline alloys with rapid quenching(RQ) and post-annealing(PA) thermal treatments are investigated by using magnetic force microscopy(MFM).The sur...The magnetic domain structures of the 100 oriented Fe 81 Ga 19 polycrystalline alloys with rapid quenching(RQ) and post-annealing(PA) thermal treatments are investigated by using magnetic force microscopy(MFM).The surfaces of the RQ alloy rods take on the dendritic domains after undergoing a standard mechanical polishing.While after PA processing,the distinct domain structures are observed at different temperatures.The wide stripe-like domain patterns appear in the surface of those PA rods at 550°C while the ramous domains remain at 400°C annealing.X-ray diffraction patterns indicate that a thin iron layer is formed on the surface of the specimens annealed at higher temperature.The soft magnetic iron layer,actually acting as a shield for the stray fields emerging from the internal magnetic structures underneath,brings about the presentation of the wide internal domains.展开更多
基金Project(10274018) supported by the National Natural Science Foundation of China project(Z200102) supported the KeyFoundation of Hebei Normal University project(2002116) supported the Foundation Education Department of of Hebei Provin
文摘FePt granular films were prepared by direct current facing-target magnetron sputtering system onto glass substrates and subsequently in-situ annealed in vacuum. Vibrating sample magnetometer, X-ray diffraction and scanning probe microscope were applied to study the magnetic properties, microstructures, morphologies and domain structures of the samples. （FePt）27Ti73 bilayer films were fabricated at various conditions to investigate the effect of Ti on FePt grains. The results show that without Ti matrix layer, FePt films deposited onto the glass substrates are fcc disordered; with addition of Ti matrix layer, FePt/Ti films form a ternary （FePt）27Ti73 alloy possessing fcc and L10 （111） mixed texture. FePt/（FePt）27Ti73 films with perfectly ordered L10（111） structure and unique magnetic properties can be obtained at Ti thickness of 35nm and substrate temperature of 250℃. The maximum coercivity is more than 240kA/m and the squareness ratio is more than 0.9. The obtained results suggest that the granular FePt/（FePt）27Ti73 films can be applicable to ultrahigh-density magnetic recording media.
文摘A new brush plating process with a soluble anode of nickel was introduced. TDY112 brush plating solution was used on the No.20 carbon steel substrate. It has the higher deposit velocity, better properties and lower cost. Scanning electronic microscopy(SEM), optical microscope, microhardness test and wear test were adopted to detect the surface quality and the properties of the coating, such as micrograph, microstructure, micro-hardness wear resistance and adherence between the coating and the substrate. The experimental results showed that the suitable technological parameters to be used, the coatings had better the surface quality, higher hardness and wear resistance.
基金Supported by the National Natural Science Foundation of China （41072153） the “Strategic Priority Research Program-Climate Change： Carbon Budget and Related Issues” of the Chinese Academy of Sciences （XDA05030100） the Foundation for University Key Teacher by Education Department of Henan Province （2009GGJS-038）.
文摘As a new technology, Atomil Force Microscopy （AFM） is being used in the research of microscopic structure on coal surface in recent years. By this technology, we can observe the nanoscale pore and crack shape of coal surface, and measure some structural parameters. Different metamorphic grades produce different feature of surface microscopic structure of coal. This paper analyzes the surface microscopic structure of different metamorphic grade coal by AFM. The results show that the coal surface microstructure has a trend from rough to smooth with the increasing of metamorphic grade. The low rank coals contain large or medium pores and the high rank coals contain micro pores. The values of surface morphology characteristic parameters （Sq and Sa） nonlinearly decrease with the increasing coal rank. That is, the coal surface becomes smoother during coalification.
文摘EPD （electrophoretic deposition） technique has been shown as an effective method to produce thin ore thick layers at voltage 5-100 V onto Ni conductive substrate. The aim of this study is to use the EPD method to fabricate films from suspensions BaTiO3. The effects of the EPD process parameters such as the suspension concentration, deposition time, electrical field strength on the specific EPD deposited weight, morphology particles were used. The surface microstructures of the as-deposited films were investigated by SEM （scanning electron microscopy）. A homogeneous microstructure was obtained at applied electric field of 100 V and I min of deposition time at an electrode distance of 1.0 cm.
文摘Objective To observe the surface structures of cardiovascular endothelial cells in situ with atomic force microscope （AFM）. Methods Fresh aorta and aortic valve were dissected from 10 healthy male New Zealand white rabbits. Before fixed in 1% formaldehyde, the fresh tissues were washed in the buffer phosphate solution. Under general microscope, the fixed aorta or valve was spread on the double side stick tape which had already been stuck on the glass slide. The intima of aorta or the aorta side of valve was towards upside, Then the specimen was dried under 37 degrees centigrade in an attemperator and was washed with pure water. After dried again, the specimen was loaded on the platform ofNanoScope Ⅲa AFM and was scanned in tapping mode with the scanning speed of 0.5 HZ. Results The surface structures of endothelial cell on the fixed and dried tissue could be observed clearly in situ with AFM. aortic endothelial cells were large, branched and arranged sparsely and parallel to the direction of blood flow, whereas endothelial cells on aorta valve surface were small, less branched and arranged intensively and vertical to the direction of blood flow. When the scanning range was dwindled, granular ultra-structures could be observed on the surface of endothelial cells, and, as the scanning range was dwindled further, fissure and convolution could be seen on the surface of granules from aortic endothelial cells. Centre cavity and surrounding swelling volcano-like structure could be seen on the surface of granules from endothelial cells of aortic valve. Conclusions It＇s feasible to observe the surface ultra-structures of cardiovascular endothelial cells in situ with AFM and morphological information provided by AFM might be of clinical value in future histopathological diagnosis（JGeriatr Cardiol2009; 6：178-181）.
基金supported partially by Hunan Provincial Science and Technology Department of China (Grant No. 2012WK3032)
文摘The magnetic domain structures of the 100 oriented Fe 81 Ga 19 polycrystalline alloys with rapid quenching(RQ) and post-annealing(PA) thermal treatments are investigated by using magnetic force microscopy(MFM).The surfaces of the RQ alloy rods take on the dendritic domains after undergoing a standard mechanical polishing.While after PA processing,the distinct domain structures are observed at different temperatures.The wide stripe-like domain patterns appear in the surface of those PA rods at 550°C while the ramous domains remain at 400°C annealing.X-ray diffraction patterns indicate that a thin iron layer is formed on the surface of the specimens annealed at higher temperature.The soft magnetic iron layer,actually acting as a shield for the stray fields emerging from the internal magnetic structures underneath,brings about the presentation of the wide internal domains.
