To determine mirror surface finishing conditions and efficient and economical superfinishing conditions for pure titanium and titanium alloys, an abrasive film is used when superfinishing is performed under varying co...To determine mirror surface finishing conditions and efficient and economical superfinishing conditions for pure titanium and titanium alloys, an abrasive film is used when superfinishing is performed under varying conditions. These conditions include the workpiece rotation speed, the oscillation speed, the contact pressure of the roller, the hardness of the roller, and the type of abrasive film. The superfinishing device is applied to polishing a thin and long cylindrical bar. A micro-finishing film and a lapping film were used as abrasive films. A1203 grains or SiC grains were used as abrasives. The surface roughness of a polished workpiece was measured using a stylus-type surface-roughness measuring instrument. As a result, the conditions to improve the polishing surface efficiently include high values for the workpiece rotation speed, oscillation speed and contact pressure. The roller hardness has no effect on the efficient polishing conditions. The mirror finish of a surface can be created using lapping film of 3 μm with Al2O3 grains after polishing to a steady surface roughness under the efficient polishing conditions.展开更多
annular beam tri-heterodyne confocal microscope has been proposed to improve the anti-environmental interference capability and the resolution of a eonfoeal microscope. It simultaneously detects far-, on-, and near-fo...annular beam tri-heterodyne confocal microscope has been proposed to improve the anti-environmental interference capability and the resolution of a eonfoeal microscope. It simultaneously detects far-, on-, and near-focus signals with given phase differences by dividing the measured light path of the eonfoeal microscope into three sub-paths (signals). Pair-wise real-time heterodyne subtraction of the three signals is used to improve the anti-environmental interference capability, axial resolution, and linearity; and a shaped annular beam super-resolution technique is used to improve lateral resolution. Theoretical analyses and preliminary experiments indicate that an axial resolution of about 1 nm can be achieved with a shaped annular beam tri-heterodyne confoeal microscope and its lateral resolution can be better than 0.2 um for A = 632.8 nm, the numerical aperture of the lens of the microscope is NA = 0.85, and the normalized radius e = 0.5.展开更多
A flexible calibration method based on a front-coated flat mirror is proposed for a laser light-sectioning three-dimensional(3D)measurement system. Since the calibration target and its mirror image are spatially separ...A flexible calibration method based on a front-coated flat mirror is proposed for a laser light-sectioning three-dimensional(3D)measurement system. Since the calibration target and its mirror image are spatially separated and can be recorded in an image by a camera,the proposed method requires only a single composite image that contains a non-planar checkerboard pattern,a laser strip projected on the target and their mirror images to complete the calibration of the camera and the laser plane in one step. Levenberg-Marquardt(LM)algorithm is used to optimize the system parameters,and the measurement accuracy and speed are improved to enable online 3D inspection. Static and dynamic online 3D measurements are carried out on a cup and a triple stepped shaft,respectively,to validate the proposed method. The shaft has two steps with the depth of(0.5±0.01)mm and(2±0.01)mm to be measured online when the shaft is rotated and translated at the same time. The measurement results can be output at a frequency of 7 to 11 readings per second with standard deviations of 0.040 mm and 0.051 mm. The experimental results verify the effectiveness and flexibility of the proposed method.展开更多
The influence of 40 kHz ultrasound radiation on the passivation behavior of zinc in 7 M KOH is presented. The results of potentiodynamic and potentiostatic measurements combined with the current oscillation caused by ...The influence of 40 kHz ultrasound radiation on the passivation behavior of zinc in 7 M KOH is presented. The results of potentiodynamic and potentiostatic measurements combined with the current oscillation caused by the irradiation were examined to explain the mechanism and the sequence of formation of the oxide films during passivation. In this study, sonication was also used to investigate both effects of the passivation duration and passivation potential on the structure of the oxide layers; the adherence of the layers was found to depend strongly on both parameters. Scanning electron microscopy-energy dispersive X-ray (SEM-EDX) analysis of the zinc surface provided complementary information on the oxide layer composition and structure.展开更多
In order to choose the appropriate reference surface on the machined surface roughness of Si Cp/Al composites, the cutting experiments of Si Cp/Al composites were carried out, and the machined surface topography was m...In order to choose the appropriate reference surface on the machined surface roughness of Si Cp/Al composites, the cutting experiments of Si Cp/Al composites were carried out, and the machined surface topography was measured by OLS3000 Confocal laser scanning microscope. The 3D measured data of machined surface topography were analyzed by the area power spectrum density. The result shows that the texture of machined surface topography in milling of Si Cp/Al composites is almost isotropic. This is the reason that the values of Rq at different locations on the same machined surface are obviously different. Through the comparison of performance of different filtering methods, the robust least squares reference surface can be used to extract the surface roughness of SiC p/Al composites effectively.展开更多
The adhesion between two parallel solid surfaces is of great interest with the rapid development of micro-nano devices and instruments.The adhesion forces between a flat tip with a diameter^1.7μm and some surface hav...The adhesion between two parallel solid surfaces is of great interest with the rapid development of micro-nano devices and instruments.The adhesion forces between a flat tip with a diameter^1.7μm and some surface have been determined by recording the force-displacement curves with an atomic force microscope(AFM).The flat tip is used to prevent wear and mimic the adhesion between two parallel surfaces.The free energy of the solid surface is calculated by the contact angles between the probe liquids and the surface.The adhesion force between parallel solid surfaces cannot be predicted by the theory of thermodynamic surface free energy.The adhesion measurements were carried out under ambient conditions,in a nitrogen-filled glove box,under distilled water,and under potassium chloride(KCl)solution.The outcome shows that the real contact area without the applied load is only a small proportion of the apparent contact area.The measurement stability and repeatability of adhesion by the AFM depend on the surface characterization,measurement methods and the environment.Under different environments,there are different interactions and factors affecting the adhesion force,and the dominant interactions and factors may be different too.The various interactions and factors are mutually coupled to determine the final adhesion force.展开更多
A new displacement measurement system is described in this paper according to the basic principles of traditional lasertriangulation method. The range of the traditional measuring method is enlarged by measuring in se...A new displacement measurement system is described in this paper according to the basic principles of traditional lasertriangulation method. The range of the traditional measuring method is enlarged by measuring in sections. Three independent CCDs, which are distributed uniformly along the optical axis, are used to achieve subsection measurement. The planemirror is regarded as a virtual detector. When imaging beam is reflected by the plane mirror, the beam is imaged on theCC D. The designed system is equivalent to add a CCD. The feasibility of the displacement measurement system is verifiedby the experiment.展开更多
Molar concentration of gold nanoparticles is one of the most critical parameters of gold colloids in order to develop their applications in sensing, diagnostics and nanomedicine. Previous methods often stand just for ...Molar concentration of gold nanoparticles is one of the most critical parameters of gold colloids in order to develop their applications in sensing, diagnostics and nanomedicine. Previous methods often stand just for gold nanoparticles with regular shape and narrow size distribution. In the present work, we proposed an absolute quantification method that determined the molar concentration of gold nanoparticles with arbitrary shapes and polydisperse sizes. This approach involved the real time monitoring and counting of individual nanoparticles collision events, from which the quantification of molar concentration was achieved using a theoretical model consisting of Fiek's laws of diffusion and Stokes-Einstein equation. The determination of spherical gold nanoparticles concentration resulted in excellent agreement with traditional spectrometry method. It was further demonstrated that the present approach can be expanded to determine the molar concentration of gold nanoparticles with arbitrary shapes and poly-diversed distributions.展开更多
基金work supported by the Second Stage of Brain Korea 21 Projects of Korea
文摘To determine mirror surface finishing conditions and efficient and economical superfinishing conditions for pure titanium and titanium alloys, an abrasive film is used when superfinishing is performed under varying conditions. These conditions include the workpiece rotation speed, the oscillation speed, the contact pressure of the roller, the hardness of the roller, and the type of abrasive film. The superfinishing device is applied to polishing a thin and long cylindrical bar. A micro-finishing film and a lapping film were used as abrasive films. A1203 grains or SiC grains were used as abrasives. The surface roughness of a polished workpiece was measured using a stylus-type surface-roughness measuring instrument. As a result, the conditions to improve the polishing surface efficiently include high values for the workpiece rotation speed, oscillation speed and contact pressure. The roller hardness has no effect on the efficient polishing conditions. The mirror finish of a surface can be created using lapping film of 3 μm with Al2O3 grains after polishing to a steady surface roughness under the efficient polishing conditions.
基金Project supported by the National Natural Science Foundation of China (Grant No 50475035), the Doctoral Program of Higher Education of China (Grant No 20050213035) and the Program for New Century Excellent Talents in University of China (Grant No NCET-05-0348).
文摘annular beam tri-heterodyne confocal microscope has been proposed to improve the anti-environmental interference capability and the resolution of a eonfoeal microscope. It simultaneously detects far-, on-, and near-focus signals with given phase differences by dividing the measured light path of the eonfoeal microscope into three sub-paths (signals). Pair-wise real-time heterodyne subtraction of the three signals is used to improve the anti-environmental interference capability, axial resolution, and linearity; and a shaped annular beam super-resolution technique is used to improve lateral resolution. Theoretical analyses and preliminary experiments indicate that an axial resolution of about 1 nm can be achieved with a shaped annular beam tri-heterodyne confoeal microscope and its lateral resolution can be better than 0.2 um for A = 632.8 nm, the numerical aperture of the lens of the microscope is NA = 0.85, and the normalized radius e = 0.5.
基金supported in part by the National Natural Science Foundation of China (No. 11802132)the Natural Science Foundation of Jiangsu Province(No.BK20180446)。
文摘A flexible calibration method based on a front-coated flat mirror is proposed for a laser light-sectioning three-dimensional(3D)measurement system. Since the calibration target and its mirror image are spatially separated and can be recorded in an image by a camera,the proposed method requires only a single composite image that contains a non-planar checkerboard pattern,a laser strip projected on the target and their mirror images to complete the calibration of the camera and the laser plane in one step. Levenberg-Marquardt(LM)algorithm is used to optimize the system parameters,and the measurement accuracy and speed are improved to enable online 3D inspection. Static and dynamic online 3D measurements are carried out on a cup and a triple stepped shaft,respectively,to validate the proposed method. The shaft has two steps with the depth of(0.5±0.01)mm and(2±0.01)mm to be measured online when the shaft is rotated and translated at the same time. The measurement results can be output at a frequency of 7 to 11 readings per second with standard deviations of 0.040 mm and 0.051 mm. The experimental results verify the effectiveness and flexibility of the proposed method.
文摘The influence of 40 kHz ultrasound radiation on the passivation behavior of zinc in 7 M KOH is presented. The results of potentiodynamic and potentiostatic measurements combined with the current oscillation caused by the irradiation were examined to explain the mechanism and the sequence of formation of the oxide films during passivation. In this study, sonication was also used to investigate both effects of the passivation duration and passivation potential on the structure of the oxide layers; the adherence of the layers was found to depend strongly on both parameters. Scanning electron microscopy-energy dispersive X-ray (SEM-EDX) analysis of the zinc surface provided complementary information on the oxide layer composition and structure.
基金Projects(51305284,61203208) supported by the National Natural Science Foundation of China
文摘In order to choose the appropriate reference surface on the machined surface roughness of Si Cp/Al composites, the cutting experiments of Si Cp/Al composites were carried out, and the machined surface topography was measured by OLS3000 Confocal laser scanning microscope. The 3D measured data of machined surface topography were analyzed by the area power spectrum density. The result shows that the texture of machined surface topography in milling of Si Cp/Al composites is almost isotropic. This is the reason that the values of Rq at different locations on the same machined surface are obviously different. Through the comparison of performance of different filtering methods, the robust least squares reference surface can be used to extract the surface roughness of SiC p/Al composites effectively.
基金国家重点研发计划(2017YFF0106404)国家自然科学基金(51675160)+4 种基金河北省应用基础研究计划重点基础研究(15961701D)河北省高层次人才资助项目(GCC2014049)河北省人才工程培养经费(A201500503)江苏省双创人才资助项目European Horizon 2020 through Marie Sklodowska-Curie Individual Fellowship Scheme(707466-3DRM)
基金supported by the National Natural Science Foundation of China(Grant No.51175182)
文摘The adhesion between two parallel solid surfaces is of great interest with the rapid development of micro-nano devices and instruments.The adhesion forces between a flat tip with a diameter^1.7μm and some surface have been determined by recording the force-displacement curves with an atomic force microscope(AFM).The flat tip is used to prevent wear and mimic the adhesion between two parallel surfaces.The free energy of the solid surface is calculated by the contact angles between the probe liquids and the surface.The adhesion force between parallel solid surfaces cannot be predicted by the theory of thermodynamic surface free energy.The adhesion measurements were carried out under ambient conditions,in a nitrogen-filled glove box,under distilled water,and under potassium chloride(KCl)solution.The outcome shows that the real contact area without the applied load is only a small proportion of the apparent contact area.The measurement stability and repeatability of adhesion by the AFM depend on the surface characterization,measurement methods and the environment.Under different environments,there are different interactions and factors affecting the adhesion force,and the dominant interactions and factors may be different too.The various interactions and factors are mutually coupled to determine the final adhesion force.
基金supported by the Science and Technology Plan of Hebei Province, China (No. 10212149)
文摘A new displacement measurement system is described in this paper according to the basic principles of traditional lasertriangulation method. The range of the traditional measuring method is enlarged by measuring in sections. Three independent CCDs, which are distributed uniformly along the optical axis, are used to achieve subsection measurement. The planemirror is regarded as a virtual detector. When imaging beam is reflected by the plane mirror, the beam is imaged on theCC D. The designed system is equivalent to add a CCD. The feasibility of the displacement measurement system is verifiedby the experiment.
基金supported by the National Natural Science Foundation of China(21405080)the Natural Science Foundation of Jiangsu Province(BK20150013,BK20140592)
文摘Molar concentration of gold nanoparticles is one of the most critical parameters of gold colloids in order to develop their applications in sensing, diagnostics and nanomedicine. Previous methods often stand just for gold nanoparticles with regular shape and narrow size distribution. In the present work, we proposed an absolute quantification method that determined the molar concentration of gold nanoparticles with arbitrary shapes and polydisperse sizes. This approach involved the real time monitoring and counting of individual nanoparticles collision events, from which the quantification of molar concentration was achieved using a theoretical model consisting of Fiek's laws of diffusion and Stokes-Einstein equation. The determination of spherical gold nanoparticles concentration resulted in excellent agreement with traditional spectrometry method. It was further demonstrated that the present approach can be expanded to determine the molar concentration of gold nanoparticles with arbitrary shapes and poly-diversed distributions.