The influence of pre-deformation on phase transformations,microstructures and hardening response in nearβTi alloy Ti5Al-3Mo-3V-2Cr-2Zr-1Nb-1Fe(wt%)during aging treatment was studied.The results show that obviousαpha...The influence of pre-deformation on phase transformations,microstructures and hardening response in nearβTi alloy Ti5Al-3Mo-3V-2Cr-2Zr-1Nb-1Fe(wt%)during aging treatment was studied.The results show that obviousαphase refinement and stronger age hardening effect can be achieved when the alloy is slightly deformed before aging treatment.Because the formation of intermediate phases(O′,ωand O′′)suppresses long-range stress induced martensitic transformation and mechanical twinning,the alloy is mainly deformed via dislocation slipping during loading.Large numbers of crystal defects are generated during predeformation.With increasing the predeformation,the number density of dislocations increases gradually.These crystal defects generated by pre-deformation may partly annihilate upon early aging,but the precipitation ofαcan also be promoted,resulting in refinedαprecipitates.In the sample with 5%pre-strain,the average thickness ofαprecipitates decreases by 57%after aging at 600℃ compared with the sample without pre-strain,and the number density increases from 7.0±1 laths/μm^(2)to 22.0±3 laths/μm^(2).Some platelet-shapedαphases form when the samples experience comparably large pre-strains such as 12%and 20%.It proves that the refinedαprecipitates and better hardening effect can be achieved by pre-deformation plus aging treatment for titanium alloy.展开更多
基金Natural Science Foundation of Shandong Province(ZR2022QE115)Liaocheng City Key Research Plan(2022YDSF85)+4 种基金Liaocheng University Doctoral Initiation Fund(318052132)Liaocheng University Students Innovation Plan(CXCY2023029)National Natrual Science Foundation of China(51671012,51671007,52174346)International Science and Technology Cooperation Program of China(2015DFA51430)Aeronautical Science Foundation of China(2015ZF51069)。
文摘The influence of pre-deformation on phase transformations,microstructures and hardening response in nearβTi alloy Ti5Al-3Mo-3V-2Cr-2Zr-1Nb-1Fe(wt%)during aging treatment was studied.The results show that obviousαphase refinement and stronger age hardening effect can be achieved when the alloy is slightly deformed before aging treatment.Because the formation of intermediate phases(O′,ωand O′′)suppresses long-range stress induced martensitic transformation and mechanical twinning,the alloy is mainly deformed via dislocation slipping during loading.Large numbers of crystal defects are generated during predeformation.With increasing the predeformation,the number density of dislocations increases gradually.These crystal defects generated by pre-deformation may partly annihilate upon early aging,but the precipitation ofαcan also be promoted,resulting in refinedαprecipitates.In the sample with 5%pre-strain,the average thickness ofαprecipitates decreases by 57%after aging at 600℃ compared with the sample without pre-strain,and the number density increases from 7.0±1 laths/μm^(2)to 22.0±3 laths/μm^(2).Some platelet-shapedαphases form when the samples experience comparably large pre-strains such as 12%and 20%.It proves that the refinedαprecipitates and better hardening effect can be achieved by pre-deformation plus aging treatment for titanium alloy.