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6种黏菌原生质团化学元素的特征 被引量:1
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作者 宋晓霞 王琦 李玉 《东北林业大学学报》 CAS CSCD 北大核心 2014年第1期112-115,121,共5页
在对黏菌绒泡菌目淡黄绒泡菌、煤绒菌、针箍菌、大孢钙皮菌、鳞钙皮菌和暗孢钙皮菌6种原生质团形态特征进行观察的基础上,利用能量色散X射线分析(EDX)技术对其冻干粉末进行化学元素组成及质量分数分析。结果表明:6种黏菌原生质团的化学... 在对黏菌绒泡菌目淡黄绒泡菌、煤绒菌、针箍菌、大孢钙皮菌、鳞钙皮菌和暗孢钙皮菌6种原生质团形态特征进行观察的基础上,利用能量色散X射线分析(EDX)技术对其冻干粉末进行化学元素组成及质量分数分析。结果表明:6种黏菌原生质团的化学元素组成及质量分数与其形态特征有密切的联系。它们共同含有C、O、Na、Mg、P、S、K、Ca 8种元素,部分含有Al、Si和Cl元素;不同物种中各元素的质量分数不同,C、Na、P和Ca元素质量分数的变化规律与6种黏菌隶属的科分类阶元有关,O、S、K、Mg质量分数与6种原生质团在统一培养条件下爬行时偏好的形态特征有关。 展开更多
关键词 黏菌 显型原生质团 形态特征 化学元素 能量色散X射线分析 ENERGY disper-sive X-RAY ANALYSIS ( EDX)
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GC-ECD检测苦荞茶中的31种农药残留不同前处理方法比较 被引量:8
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作者 邱世婷 侯雪 +2 位作者 杨晓凤 韩梅 赵郭艳 《云南农业大学学报(自然科学版)》 CSCD 北大核心 2017年第3期536-542,共7页
【目的】以气相色谱—电子捕获检测器(GC-ECD)技术为基础,建立了适合苦荞茶中31种农药残留分析的4种前处理方法:SPE(florisil柱)法、SPE(NH_2-Carb柱)法、GPC法、d-SPE(PSA+C18)法。【方法】以苦荞茶中的有机氯和拟除虫菊酯类等共31种... 【目的】以气相色谱—电子捕获检测器(GC-ECD)技术为基础,建立了适合苦荞茶中31种农药残留分析的4种前处理方法:SPE(florisil柱)法、SPE(NH_2-Carb柱)法、GPC法、d-SPE(PSA+C18)法。【方法】以苦荞茶中的有机氯和拟除虫菊酯类等共31种农药为研究对象,从空白基质净化效果、基质效应、不同浓度添加回收率方面对4种前处理方式进行对比分析。【结果】SPE(florisil柱)法得到的空白基质干扰最少,基质效应最弱,稳定性最好,能保证大部分目标物的回收率在70%~120%,但对氟虫腈及代谢物回收率较差;SPE(NH_2-Carb柱)法能保证氟虫腈及其代谢物和大部分目标化合物的回收率,适合于多农药残留分析检测,但对环境不友好;GPC法稳定性略差;d-SPE(PSA+C18)法方法简便快捷,但回收率偏高,应配合内标法或对分散固相萃取剂用量进一步优化后使用。【结论】本研究可为苦荞茶中31种农药残留测定方法的选择提供数据支持。 展开更多
关键词 苦荞茶 固相小柱萃取 凝胶渗透法 分散固相萃取 GC—ECD 农药残留
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Mineral Particles Found on the Hairs of Holy Maria-Magdalena Studied by Scanning Electron Microscopy and Elemental Analysis
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作者 Gérard Lucotte 《Open Journal of Applied Sciences》 2020年第3期41-59,共19页
The presumed hairs of Holy Maria-Magdalena are studied here for mineral particles found on their surfaces, by the techniques of scanning electron microscopy coupled with energy dispersive X-ray. Exploration by these t... The presumed hairs of Holy Maria-Magdalena are studied here for mineral particles found on their surfaces, by the techniques of scanning electron microscopy coupled with energy dispersive X-ray. Exploration by these techniques of the hair surfaces allows us to observe and study some marble fragments that can originate from the walls of the sarcophagus in which Maria-Magdalena’s remains were kept. These new findings support the authenticity of the hair as traditionally reported in the French “tradition des Saints de Provence”. 展开更多
关键词 Maria-Magdalena’s HAIR Scanning Electron Microscopy Energy disper-sive X-Ray MARBLE FRAGMENTS MINERAL Particles
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Transfer characteristics of dynamic biochemical signals in non-reversing pulsatile flows in a shallow Y-shaped microfluidic channel: signal filtering and nonlinear amplitude-frequency modulation
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作者 Zongzheng CHEN Weimo YUAN +4 位作者 A.R.AZIZ Zhengming GAO Depei ZENG Bo LIU Kairong QIN 《Applied Mathematics and Mechanics(English Edition)》 SCIE EI CSCD 2017年第10期1481-1496,共16页
The transports of the dynamic biochemical signals in the non-reversing pulsatile flows in the mixing microchannel of a Y-shaped microfluidic device are ana- lyzed. The results show that the mixing micro-channel acts a... The transports of the dynamic biochemical signals in the non-reversing pulsatile flows in the mixing microchannel of a Y-shaped microfluidic device are ana- lyzed. The results show that the mixing micro-channel acts as a low-pass filter, and the biochemical signals are nonlinearly modulated by the pulsatile flows, which depend on the biochemical signal frequency, the flow signal frequency, and the biochemical signal transporting distance. It is concluded that, the transfer characteristics of the dynamic biochemical signals, which are transported in the time-varying flows, should be carefully considered for better loading biochemical signals on the cells cultured on the bottom of the microfluidic channel. 展开更多
关键词 shallow Y-shaped microfluidic channel dynamic biochemical signal non-reversing pulsatile flow nonlinear amplitude-frequency modulation Taylor-Aris disper-sion
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Stability and dispersion analysis of reproducing kernel collocation method for transient dynamics
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作者 罗汉中 刘学文 黄醒春 《Applied Mathematics and Mechanics(English Edition)》 SCIE EI 2011年第6期777-788,共12页
A reproducing kernel collocation method based on strong formulation is introduced for transient dynamics. To study the stability property of this method, an algorithm based on the von Neumann hypothesis is proposed to... A reproducing kernel collocation method based on strong formulation is introduced for transient dynamics. To study the stability property of this method, an algorithm based on the von Neumann hypothesis is proposed to predict the critical time step. A numerical test is conducted to validate the algorithm. The numerical critical time step and the predicted critical time step are in good agreement. The results are compared with those obtained based on the radial basis collocation method, and they axe in good agreement. Several important conclusions for choosing a proper support size of the reproducing kernel shape function are given to improve the stability condition. 展开更多
关键词 reproducing kernel collocation method (RKCM) stability analysis disper-sion analysis transient dynamics
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Effect of Copper Content on the Direct Process of Organosilane Synthesis from Silicon and Methyl Chloride 被引量:4
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作者 罗务习 张国良 +1 位作者 王光润 王金福 《Tsinghua Science and Technology》 SCIE EI CAS 2006年第2期252-258,共7页
The effect of copper concentration on the performance of the catalytic reaction between silicon and methyl chloride was investigated using online gas chromatogram. The catalyst concentration greatly influences various... The effect of copper concentration on the performance of the catalytic reaction between silicon and methyl chloride was investigated using online gas chromatogram. The catalyst concentration greatly influences various aspects of the direct organosilane synthesis process, including the reaction rate, the selec- tivity, and the silicon conversion. The reaction activity and the silicon conversion increase as the catalyst concentration increases. However, the reaction selectivity decreases for the catalyst concentrations more .than 9 wt.%. The cross-sections of deactivated contact mass particles were observed by optical microscopy and analyzed by scanning electron microscope combined with energy dispersive X-ray detector (SEM-EDX) The observations showed that a textured substance formed on the original flat surface of the silicon particles after deactivation with copper only in a shallow surface layer of the contact mass. This indicates that the copper diffusion is the rate limiting step which causes the reaction deactivation. 展开更多
关键词 direct process copper concentration reaction activity reaction selectivity silicon conversion online gas chromatogram (GC) scanning electron microscope combined with energy disper-sive X-ray detector (SEM-EDX)
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A Weighted Runge-Kutta Discontinuous Galerkin Method for 3D Acoustic and Elastic Wave-Field Modeling 被引量:2
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作者 Xijun He Dinghui Yang Xiao Ma 《Communications in Computational Physics》 SCIE 2020年第6期372-400,共29页
Numerically solving 3D seismic wave equations is a key requirement for forward modeling and inversion.Here,we propose a weighted Runge-Kutta dis-continuous Galerkin(WRKDG)method for 3D acoustic and elastic wave-field ... Numerically solving 3D seismic wave equations is a key requirement for forward modeling and inversion.Here,we propose a weighted Runge-Kutta dis-continuous Galerkin(WRKDG)method for 3D acoustic and elastic wave-field mod-eling.For this method,the second-order seismic wave equations in 3D heteroge-neous anisotropic media are transformed into a first-order hyperbolic system,and then we use a discontinuous Galerkin(DG)solver based on numerical-flux formulations for spatial discretization.The time discretization is based on an implicit di-agonal Runge-Kutta(RK)method and an explicit iterative technique,which avoids solving a large-scale system of linear equations.In the iterative process,we introduce a weighting factor.We investigate the numerical stability criteria of the 3D method in detail for linear and quadratic spatial basis functions.We also present a 3D analysis of numerical dispersion for the full discrete approximation of acoustic equation,which demonstrates that the WRKDG method can efficiently suppress numerical dispersion on coarse grids.Numerical results for several different 3D models including homogeneous and heterogeneous media with isotropic and anisotropic cases show that the 3D WRKDG method can effectively suppress numerical dispersion and provide accurate wave-field information on coarse mesh. 展开更多
关键词 Numerical modeling ANISOTROPY discontinuous Galerkin method numerical disper-sion STABILITY
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Generation and transmission RZ-OOK signal for of dispersion tolerant lO-Gbps radio over fiber link
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作者 Yousaf KHAN Xiangjun XIN ARab HUSSAIN Liu BO Shahryar SHAFIQUE 《Frontiers of Optoelectronics》 2012年第3期306-310,共5页
We proposed and demonstrated the generation and transmission of 10-Gbps retum-to-zero ON/OFF keying (RZ-OOK) signal using a new technique without pulse carving at transmitter. The new technique is characterized by a... We proposed and demonstrated the generation and transmission of 10-Gbps retum-to-zero ON/OFF keying (RZ-OOK) signal using a new technique without pulse carving at transmitter. The new technique is characterized by a 3 dB built-in gain with better tolerance for chromatic dispersion in standard single mode fiber (SSMF). Fiber Bragg grating (FBG) is used as chromatic dispersion compensating device to investigate the toler- ance of the proposed scheme. The simulation model of wavelength division multiplexing (WDM) based on OptiSystem.v.8.0 is presented. Simulation results show that there are error free transmission performance in a distance of 600 km with negligible power penalty and improved receiver sensitivity compared to conventional pulse carving approach. 展开更多
关键词 modulation pulse carver chromatic disper-sion fiber Bragg gratings radio over fiber (RoF)
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Effects of polyethylenimine on the dispersibility of hollow silica nanoparticles
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作者 WEN Lixiong WANG Qing +1 位作者 ZHENG Tianyuan CHEN Jianfeng 《Frontiers of Chemical Science and Engineering》 SCIE EI CSCD 2007年第3期277-282,共6页
In this study,two different methods were applied to disperse hollow silica nanoparticles(HSNP);one employed polyethylenimine(PEI)as the dispersant during the synthesis processes for preparing HSNP,while the other adde... In this study,two different methods were applied to disperse hollow silica nanoparticles(HSNP);one employed polyethylenimine(PEI)as the dispersant during the synthesis processes for preparing HSNP,while the other added PEI into suspensions of the prepared HSNP and used milling treatment to achieve the desired dispersion.It was found that adding PEI during the synthesis process of HSNP had no noticeable improvement in the dispersion,while adding PEI into suspen-sions of the prepared HSNP and utilizing milling treatment resulted in remarkable dispersion improvement.Therefore,the latter was chosen as the method in dispersing HSNP suspensions.The adsorption of PEI on the surface of HSNP and the stability of the aqueous suspensions was investigated.The results indicated that the adsorption of PEI on the surface of HSNP would increase the repulsive energy among particles,hence reducing the agglomeration of HSNP and improving the stability of the aqueous suspensions.The change of HSNP’s ■ potential after adding PEI and the rela-tionship between the adsorbed amount of PEI and pH were also investigated. 展开更多
关键词 hollow silica nano-particles(HSNP) disper-sion polyethylenimine(PEI) ■potential adsorption
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