以TC4-DT钛合金为研究对象,研究不同温度(20,300,500℃)对TC4-DT的摩擦磨损性能的影响。采用HT-500型摩擦磨损试验机对TC4-DT合金进行摩擦磨损实验,分析温度对摩擦因数及磨损率的影响;通过扫描电镜(Scanning electron microscope,SEM)...以TC4-DT钛合金为研究对象,研究不同温度(20,300,500℃)对TC4-DT的摩擦磨损性能的影响。采用HT-500型摩擦磨损试验机对TC4-DT合金进行摩擦磨损实验,分析温度对摩擦因数及磨损率的影响;通过扫描电镜(Scanning electron microscope,SEM)和能谱(Energy dispersive spectrometer,EDS)等方法探究磨痕的形貌和成分变化及磨损机理。结果表明,随着温度的升高,磨损过程中TC4-DT合金表面不断生成氧化膜,摩擦因数从0.493下降到0.298,磨痕不断变窄变浅,磨损率大大降低;磨损机理在20℃时以粘着磨损、磨粒磨损为主,伴随着疲劳磨损;在300,500℃时以剥层磨损和氧化磨损为主,伴随少量的粘着磨损和磨粒磨损。展开更多
Influence of thermomechanical treatments （mill annealing, duplex annealing, solution treatment plus aging and triple annealing） on microstructures and mechanical properties of TC4-DT titanium alloy was investigated....Influence of thermomechanical treatments （mill annealing, duplex annealing, solution treatment plus aging and triple annealing） on microstructures and mechanical properties of TC4-DT titanium alloy was investigated. Results showed that thermomechanical treatments had a significant influence on the microstructure parameters and higher annealing and aging temperature and lower cooling rate led to the decrease of the volume fraction of primaryαand the size of prior-βand the increase of the width of grain boundary αand secondary α. The highest strength was obtained by solution treatment and aging due to a large amount of transformedβand finer grain boundaryαand secondaryαat the expense of slight decrease of elongation and the ultimate strength, yield strength, elongation, reduction of area were 1100 MPa, 1030 MPa, 13%and 53%separately. A good combination of strength and ductility has been obtained by duplex annealing with the above values 940 MPa, 887.5 MPa, 15%and 51%respectively. Analysis between microstructure parameters and tensile properties showed that with the volume fraction of transformedβphase and the prior-βgrain size increasing, the ultimate strength, yield strength and reduction of area increased, but the elongation decreased. While the width of grain boundary α and secondary α showed a contrary effect on the tensile properties. Elimination of grain boundaryαas well as small prior-βgrain size can also improve ductility.展开更多
TC4-DT钛合金经高温恒应变速率变形后,进行三重热处理,具体工艺为：（920~960℃）×1 h水冷（WQ）＋（880~920）℃×1h WQ＋820℃×1.5 h空冷（AC）,观察热处理后的微观组织。结果表明：TC4-DT钛合金950℃变形后,第一重热...TC4-DT钛合金经高温恒应变速率变形后,进行三重热处理,具体工艺为：（920~960℃）×1 h水冷（WQ）＋（880~920）℃×1h WQ＋820℃×1.5 h空冷（AC）,观察热处理后的微观组织。结果表明：TC4-DT钛合金950℃变形后,第一重热处理温度越高,初生等轴α相含量越少,在温度为920℃时由等轴α相、针状α＇相及β基体组成,960℃时等轴α相完全消失;第二重热处理中,初生α相有减少的趋势,温度越高,减少越快。第二重热处理温度对次生条状α相含量及最终形态也有影响,当二重热温度为920℃时得到的条状α组织更为粗大;经过第三重热处理,条状α相的间距均匀,在条状一次次生α相之间分布有更加细小的二次次生α相。因而采用不同条件的多重热处理制度可以调节材料的微观组织,包括次生α的长度、宽度及次生α片层的数量等,从而可以优化TC4-DT钛合金的微观组织。TC4-DT钛合金950℃高温变形后,经960℃×1 h WQ＋880℃×1 h WQ＋820℃×1.5 h AC热处理,得到细小均匀的网篮组织;经940℃×1 h WQ＋920℃×1 h WQ＋820℃×1.5 h AC热处理,得到双态组织。展开更多
文摘以TC4-DT钛合金为研究对象,研究不同温度(20,300,500℃)对TC4-DT的摩擦磨损性能的影响。采用HT-500型摩擦磨损试验机对TC4-DT合金进行摩擦磨损实验,分析温度对摩擦因数及磨损率的影响;通过扫描电镜(Scanning electron microscope,SEM)和能谱(Energy dispersive spectrometer,EDS)等方法探究磨痕的形貌和成分变化及磨损机理。结果表明,随着温度的升高,磨损过程中TC4-DT合金表面不断生成氧化膜,摩擦因数从0.493下降到0.298,磨痕不断变窄变浅,磨损率大大降低;磨损机理在20℃时以粘着磨损、磨粒磨损为主,伴随着疲劳磨损;在300,500℃时以剥层磨损和氧化磨损为主,伴随少量的粘着磨损和磨粒磨损。
基金Project(51101119)supported by the National Natural Science Foundation of China
文摘Influence of thermomechanical treatments （mill annealing, duplex annealing, solution treatment plus aging and triple annealing） on microstructures and mechanical properties of TC4-DT titanium alloy was investigated. Results showed that thermomechanical treatments had a significant influence on the microstructure parameters and higher annealing and aging temperature and lower cooling rate led to the decrease of the volume fraction of primaryαand the size of prior-βand the increase of the width of grain boundary αand secondary α. The highest strength was obtained by solution treatment and aging due to a large amount of transformedβand finer grain boundaryαand secondaryαat the expense of slight decrease of elongation and the ultimate strength, yield strength, elongation, reduction of area were 1100 MPa, 1030 MPa, 13%and 53%separately. A good combination of strength and ductility has been obtained by duplex annealing with the above values 940 MPa, 887.5 MPa, 15%and 51%respectively. Analysis between microstructure parameters and tensile properties showed that with the volume fraction of transformedβphase and the prior-βgrain size increasing, the ultimate strength, yield strength and reduction of area increased, but the elongation decreased. While the width of grain boundary α and secondary α showed a contrary effect on the tensile properties. Elimination of grain boundaryαas well as small prior-βgrain size can also improve ductility.
文摘TC4-DT钛合金经高温恒应变速率变形后,进行三重热处理,具体工艺为：（920~960℃）×1 h水冷（WQ）＋（880~920）℃×1h WQ＋820℃×1.5 h空冷（AC）,观察热处理后的微观组织。结果表明：TC4-DT钛合金950℃变形后,第一重热处理温度越高,初生等轴α相含量越少,在温度为920℃时由等轴α相、针状α＇相及β基体组成,960℃时等轴α相完全消失;第二重热处理中,初生α相有减少的趋势,温度越高,减少越快。第二重热处理温度对次生条状α相含量及最终形态也有影响,当二重热温度为920℃时得到的条状α组织更为粗大;经过第三重热处理,条状α相的间距均匀,在条状一次次生α相之间分布有更加细小的二次次生α相。因而采用不同条件的多重热处理制度可以调节材料的微观组织,包括次生α的长度、宽度及次生α片层的数量等,从而可以优化TC4-DT钛合金的微观组织。TC4-DT钛合金950℃高温变形后,经960℃×1 h WQ＋880℃×1 h WQ＋820℃×1.5 h AC热处理,得到细小均匀的网篮组织;经940℃×1 h WQ＋920℃×1 h WQ＋820℃×1.5 h AC热处理,得到双态组织。
