Effect of Gd Addition on Hot Deformation Behavior and Microstructure Evolution of 7075 Aluminum Alloy

In order to clarify the effect of rare earth Gd on the microstructure evolution and deformation behavior of 7075 aluminum alloy during hot compression,uniaxial compression tests of Al-Zn-Mg-Cu-0.5%Gd were conducted at strain rates of 0.001,0.01,0.1,and 1 s^(-1)with the temperatures ranging from 350 to 450℃.The microstructural evolution during deformation was characterized using optical microscopy and electron backscatter diffraction(EBSD)techniques.The experimental results indicate that the addition of the rare earth element Gd significantly increases the peak flow stress and thermal activation energy of the alloy.Due to the pinning effect of rare earth phases,dislocation movement is hindered,leading to an increased level of work hardening in the alloy.However,the dynamic recrystallization of the alloy is complicated.At a high Z(Zener-Hollomon parameter)values,recrystallization occurs in the form of DDRX(Discontinuous Dynamic Recrystallization),making it easier to nucleate at grain boundaries.As the Z value decreases gradually,the recrystallization mechanism transitions from discontinuous dynamic recrystallization(DDRX)to continuous dynamic recrystallization(CDRX).At a low Z values with the strain rate of 0.001 s^(-1),the inhibitory effect of rare earths weakens,resulting in a comparable recrystallization ratio between Al-Zn-Mg-Cu-Gd alloy and 7075 aluminum alloy.Moreover,the average grain size of the aluminum alloy with Gd addition is only half that of 7075 aluminum.The addition of Gd provides Orowan and substructure strengthening for the alloy,which greatly improves the work-hardening of the alloy compared with 7075 aluminum alloy and improves the strength of the alloy.

Enhancing constitutive description and workability characterization of Mg alloy during hot deformation using machine learning-based Arrhenius-type model

Hot deformation is a commonly employed processing technique to enhance the ductility and workability of Mg alloy.However,the hot deformation of Mg alloy is highly sensitive to factors such as temperature,strain rate,and strain,leading to complex flow behavior and an exceptionally narrow processing window for Mg alloy.To overcome the shortcomings of the conventional Arrhenius-type(AT)model,this study developed machine learning-based Arrhenius-type(ML-AT)models by combining the genetic algorithm(GA),particle swarm optimization(PSO),and artificial neural network(ANN).Results indicated that when describing the flow behavior of the AQ80 alloy,the PSO-ANN-AT model demonstrates the most prominent prediction accuracy and generalization ability among all ML-AT and AT models.Moreover,an activation energy-processing(AEP)map was established using the reconstructed flow stress and activation energy fields based on the PSO-ANN-AT model.Experimental validations revealed that this AEP map exhibits superior predictive capability for microstructure evolution compared to the one established by the traditional interpolation methods,ultimately contributing to the precise determination of the optimum processing window.These findings provide fresh insights into the accurate constitutive description and workability characterization of Mg alloy during hot deformation.

Hot Deformation Behavior of Ti-6Al-4V-0.5Ni-0.5Nb Titanium Alloy

Characterization of hot deformation behavior of Ti-6Al-4V-0.5Ni-0.5Nb titanium alloy was investigated through isothermal compression at various temperatures from 750 to 1050℃and strain rate from 0.01 to 10 s^(-1).The isothermal compression experiment results showed that the peak stress of Ti-6Al-4V-0.5Ni-0.5Nb titanium alloy decreased with the temperature increasing and the strain rate decreasing.The softening mechanism was dynamic recovery below T_(β)and changed to dynamic recrystallization above T_(β).The arrheniustype relationship was used to calculate the constitutive equation of Ti-6Al-4V-0.5Ni-0.5Nb alloy in two-phase regions.It was found that the apparent activation energies were 427.095 kJ·mol^(-1)in theα+βphase region and 205.451 kJ·mol^(-1)in theβphase region,respectively.On the basis of dynamic materials model,the processing map is generated,which shows that the highest peak efficiency of power dissipation of 56%occurs at about 1050℃/0.01 s^(-1).It can be found in the processing maps that the strain had significant effect on the peak region of power dissipation efficiency of Ti-6Al-4V-0.5Ni-0.5Nb alloy.Furthermore,optimized hot working regions were investigated and validated through microstructure observation.The optimum thermo mechanical process condition for hot working of Ti-6Al-4V-0.5Ni-0.5Nb titanium alloy was suggested to be in the temperature range of 950-1000℃with a strain rate of 0.01-0.1 s^(-1).

Prediction of Hot Deformation Behavior of 7Mo Super Austenitic Stainless Steel Based on Back Propagation Neural Network

The hot compression tests of 7Mo super austenitic stainless(SASS)were conducted to obtain flow curves at the temperature of 1000-1200℃and strain rate of 0.001 s^(-1)to 1 s^(-1).To predict the non-linear hot deformation behaviors of the steel,back propagation-artificial neural network(BP-ANN)with 16×8×8 hidden layer neurons was proposed.The predictability of the ANN model is evaluated according to the distribution of mean absolute error(MAE)and relative error.The relative error of 85%data for the BP-ANN model is among±5%while only 42.5%data predicted by the Arrhenius constitutive equation is in this range.Especially,at high strain rate and low temperature,the MAE of the ANN model is 2.49%,which has decreases for 18.78%,compared with conventional Arrhenius constitutive equation.

Hot deformation behavior of Fe–27.34Mn–8.63Al–1.03C lightweight steel

Hot compression tests were performed to investigate the hot deformation behavior of Fe–27.34Mn–8.63Al–1.03C lightweight steel and optimize the hot workability parameters. The temperature range was 900–1150℃ and the strain rate range was 0.01–5 s^(-1)on a Gleeble-3800 thermal simulator machine. The results showed that the flow stress increased with decreasing deformation temperature and increasing strain rate. According to the constitutive equation, the activation energy of hot deformation was 422.88 kJ·mol^(-1). The relationship between the critical stress and peak stress of the tested steel was established, and a dynamic recrystallization kinetic model was thus obtained. Based on this model, the effects of strain rate and deformation temperature on the volume fraction of dynamically recrystallized grains were explored. The microstructural examination and processing map results revealed that the tested steel exhibited a good hot workability at deformation temperatures of 1010–1100℃ and strain rate of 0.01 s^(-1).

Influence of rare earth Ce on hot deformation behavior of as-cast Mn18Cr18N high nitrogen austenitic stainless steel

The hot deformation behavior of Mn18Cr18N and Mn18Cr18N+Ce high nitrogen austenitic stainless steels at 1173-1473 K and 0.01-1 s^(-1) were investigated by thermal compression tests.The influence mechanism of Ce on the hot deformation behavior was analyzed by Ce-containing inclusions and segregation of Ce.The results show that after the addition of Ce,large,angular,hard,and brittle inclusions(TiN-Al_(2)O_(3),TiN,and Al_(2)O_(3)) can be modified to fine and dispersed Ce-containing inclusions(Ce-Al-O-S and TiN-Ce-Al-O-S).During the solidification,Ce-containing inclusions can be used as heterogeneous nucleation particles to refine as-cast grains.During the hot deformation,Ce-containing inclusions can pin dislocation movement and grain boundary migration,induce dynamic recrystallization(DRX)nucleation,and avoid the formation and propagation of micro cracks and gaps.In addition,during the solidification,Ce atoms enrich at the front of solid-li-quid interface,resulting in composition supercooling and refining the secondary dendrites.Similarly,during the hot deformation,Ce atoms tend to segregate at the boundaries of DRX grains,inhibiting the growth of grains.Under the synergistic effect of Ce-containing inclusions and Ce segregation,although the hot deformation resistance and hot deformation activation energy are improved,DRX is more likely to occur and the size of DRX grains is significantly refined,and the problem of hot deformation cracking can be alleviated.Finally,the microhardness of the samples was measured.The results show that compared with as-cast samples,the microhardness of hot-deformed samples increases signific-antly,and with the increase of DRX degree,the microhardness decreases continuously.In addition,Ce can affect the microhardness of Mn18Cr18N steel by affecting as-cast and hot deformation microstructures.

Study on hot deformation behavior of homogenized Mg-8.5Gd-4.5Y-0.8Zn-0.4Zr alloy using a combination of strain-compensated Arrhenius constitutive model and finite element simulation method

Isothermal hot compression experiments were conducted on homogenized Mg-8.5Gd-4.5Y-0.8Zn-0.4Zr alloy to investigate hot deformation behavior at the temperature range of 673-773 K and the strain rate range of 0.001-1 s^(-1)by using a Gleeble-1500D thermo mechanical simulator.Metallographic characterization on samples deformed to true strain of 0.70 illustrates the occurrence of flow localization and/or microcrack at deformation conditions of 673 K/0.01 s^(-1),673 K/1 s^(-1)and 698 K/1 s^(-1),indicating that these three deformation conditions should be excluded during hot working of homogenized Mg-8.5Gd-4.5Y-0.8Zn-0.4Zr alloy.Based on the measured true stress-strain data,the strain-compensated Arrhenius constitutive model was constructed and then incorporated into UHARD subroutine of ABAQUS software to study hot deformation process of homogenized Mg-8.5Gd-4.5Y-0.8Zn-0.4Zr alloy.By comparison with measured force-displacement curves,the predicted results can describe well the rheological behavior of homogenized Mg-8.5Gd-4.5Y-0.8Zn-0.4Zr alloy,verifying the validity of finite element simulation of hot compression process with this complicated constitutive model.Numerical results demonstrate that the distribution of values of material parameters(α,n,Q and ln A)within deformed sample is inhomogeneous.This issue is directly correlated to the uneven distribution of equivalent plastic strain due to the friction effect.Moreover,at a given temperature the increase of strain rate would result in the decrease of equivalent plastic strain within the central region of deformed sample,which hinders the occurrence of dynamic recrystallization(DRX).

Hot deformation behavior of novel high-strength Mg-0.6Mn-0.5Al-0.5Zn-0.4Ca alloy

The hot compression behavior of as-extruded Mg-0.6Mn-0.5Al-0.5Zn-0.4Ca alloy was studied on a Gleeble-3500 thermal simulation machine.Experiments were conducted at temperatures ranging from 523 to 673 K and strain rates ranging from 0.001 to 1 s^(-1).Results showed that an increase in the strain rate or a decrease in deformation temperature led to an increase in true stress.The constitutive equation and processing maps of the alloy were obtained and analyzed.The influence of deformation temperatures and strain rates on microstructural evolution and texture was studied with the assistance of electron backscatter diffraction(EBSD).The as-extruded alloy exhibited a bimodal structure that consisted of deformed coarse grains and fine equiaxed recrystallized structures(approximately 1.57μm).The EBSD results of deformed alloy samples revealed that the recrystallization degree and average grain size increased as the deformation temperature increased.By contrast,dislocation density and texture intensity decreased.Compressive texture weakened with the increase in the deformation temperature at the strain rate of 0.01 s-1.Most grains with{0001}planes tilted away from the compression direction(CD)gradually.In addition,when the strain rate decreased,the recrystallization degree and average grain size increased.Meanwhile,the dislocation density decreased.Texture appeared to be insensitive to the strain rate.These findings provide valuable insights into the hot compression behavior,microstructural evolution,and texture changes in the Mg-0.6Mn-0.5Al-0.5Zn-0.4Ca alloy,contributing to the understanding of its processing-microstructure-property relationships.

Hot deformation behavior and microstructure evolution of Be/2024Al composites

The high temperature compression test of Be/2024Al composites with 62wt%Be was conducted at 500–575℃ and strain rate of0.003–0.1 s^(-1).The strain-compensated Arrhenius model and modified Johnson–Cook model were introduced to predict the hot deformation behavior of Be/2024Al composites.The result shows that the activation energy of Be/2024Al composites was 363.364 k J·mol^(-1).Compared with composites reinforced with traditional ceramics,Be/2024Al composites can be deformed with ultra-high content of reinforcement,attributing to the deformable property of Be particles.The average relative error of the two models shows that modified Johnson–Cook model was more suitable for low temperature condition while strain-compensated Arrhenius model was more suitable for high temperature condition.The processing map was generated and a hot extrusion experiment was conducted according to the map.A comparation of the microstructure of Be/2024Al composites before and after extrusion shows that the Be particle deformed coordinately with the matrix and elongated at the extrusion direction.

Modeling of strain hardening and dynamic recrystallization of ZK60 magnesium alloy during hot deformation

The flow stress behavior of ZK60 alloy at elevated temperature was investigated. The strain hardening and dynamic recrystallization of the alloy were modeled by Kocks-Meching model and Avrami equation, respectively. A new constitutive equation during hot deformation was constructed to predict the flow stress considering the dynamic recrystallization. The results show that the flow stress curves predicted by the proposed equation have high correlation coefficients with the experimental data, which confirms that the developed model is accurate and effective to establish the flow stress equation of ZK60 magnesium alloy during hot deformation. Microstructure observation shows that dynamic recovery occurs in the initial stage of hot deformation. However, the microstructure turns to recrvstallization structure as the strain increases.

Hot deformation behavior of extruded AZ80 magnesium alloy

The hot deformation behavior of extruded AZ80 magnesium alloy was studied through hot compression tests performed at temperatures ranging from 250 to 450 ~C with strain rates varying from 0.001 to 10 s-1. The flow stress was corrected due to the deformation heating. The Zener-Hollomon parameter （Z parameter） and processing map were established to describe the hot deformation behavior. The results indicate that the applicable deformation should be conducted at the strain rate of 0.1 s-~ and the temperature range of 350-400 ~C. Besides, the relationship between the microstructure evolution and Z parameter was also discussed. High temperature and low strain rate result in a low Z parameter, which leads to full dynamic recrystallization （DRX） and large DRX grain size in the microstructure. Considering processing map and microstructure, the hot deformation should be carried out at the temperature of 400 ~C and the strain rate of 0.1 s 1.

Effect of hot deformation conditions on grain structure and properties of 7085 aluminum alloy

The influences of deformation conditions on grain structure and properties of 7085 aluminum alloy were investigated by optical microscopy and transmission electron microscopy in combination with tensile and fracture toughness tests. The results show that the volume fraction of dynamic recrystallization increased with the decrease of Zener-Hollomon （Z） parameter, and the volume fraction of static recrystallization increased with the increasing of Z parameter. The strength and fracture toughness of the alloy after solution and aging treatment first increased and then decreased with the increase of Z parameter. The microstructure map was established on the basis of microstructure evolution during deformation and solution heat treatment. The optimization deformation conditions were acquired under Z parameters of 1.2×10^10-9.1×10^12.

Hot deformation behavior and microstructural evolution of beta C titanium alloy in β phase field

The hot deformation behavior of beta C titanium alloy in β phase field was investigated by isothermal compression testson a Gleeble？3800 thermomechanical simulator. The constitutive equation describing the hot deformation behavior was obtained anda processing map was established at the true strain of 0.7. The microstructure was characterized by optical microscopy （OM）,scanning electron microscopy （SEM） and electron back-scattered diffraction （EBSD） technique. The results show that the flow stressincreases with increasing strain rates, and decreases with increasing experimental temperatures. The calculated apparent activationenergy （167 kJ/mol） is close to that of self-diffusion in β titanium. The processing map and microstructure observation exhibit adynamic recrystallization domain in the temperature range of 900-1000 ℃ and strain rate range of 0.1-1 s^-1. An instability regionexists when the strain rate is higher than 1.7 s^-1. The microstructure of beta C titanium alloy can be optimized by proper heattreatments after the deformation in the dynamic recrystallization domain.

Hot deformation behavior of TC11/Ti-22Al-25Nb dual-alloy in isothermal compression

The high-temperature flow behavior of TCll/Ti-22Al-25 Nb electron beam（EB） weldments was investigated by the isothermal compression tests at the temperature of 900-1060℃ and the strain rate of 0.001-10 s-（-1）.Based on the experimental data,the constitutive equation that describes the flow stress as a function of strain rate and deformation temperature is obtained.The apparent activation energy of deformation is calculated,which decreases with increasing the strain and the value is 334 kJ/mol at strain of 0.90.The efficiency of power dissipation η changes obviously with the variation of deformation conditions.Under the strain rates of 0.01,0.1 and 1 s-（-1）,the value of η increases with increasing the true strain for different deformation temperatures.While the value of η decreases with increasing the strain under the strain rates of 0.001 and 10 s-（-1）.The optimum processing condition is（t（opi）=1060℃,ε（opi）=0.1 s-（-1）） with the peak efficiency of 0.51.Under this deformation,dynamic recrystallization（DRX） is observed obviously in the microstructure of welding zone.Under the condition of 1060℃ and 0.001 s-（-1）,the deformation mechanism is dominated by dynamic recovery（DRV） and the value of η decreases sharply（η=0.02）.The flow instability is predicted to occur since the instability parameter ξ（ε）becomes negative.The hot working process can be carried out safely in the domain with the strain rate of 0.001-0.6 s-（-1） and the temperature of 900-1060℃.

Rate controlling mechanisms in hot deformation of 7A55 aluminum alloy

The hot deformation behavior of 7A55 aluminum alloy was investigated at the temperature ranging from 300 ℃ to 450 ℃ and strain rate ranging from 0.01 s-1 to 1 s-1 on a Gleeble-3500 simulator. Processing maps were established in order to apprehend the kinetics of hot deformation and the rate controlling mechanism was interpreted by the kinetic rate analysis obeying power-law relation. The results indicated that one significant domain representing dynamic recrystallization （DRX） existed on the processing maps and lying in 410-450 ＆#176;C and 0.05-1 s-1. The conclusions of kinetic analysis correlated well with those obtained from processing maps. The apparent activation energy values calculated in the dynamic recrystallization （DRX） domain and the stability regions except dynamic recrystallization （DRX） domain were 91.2 kJ/mol and 128.8 kJ/mol, respectively, which suggested that grain boundary self-diffusion and cross-slip were the rate controlling mechanisms.

Microstructure and magnetic properties of anisotropic Nd-Fe-B magnets prepared by spark plasma sintering and hot deformation

Bulk anisotropic Nd-Fe-B magnets were prepared from hydrogen-disproportionation-desorption-recombination（HDDR） powders via spark plasma sintering（SPS） and subsequent hot deformation. The influence of sintering temperature on the structure and magnetic properties of the spark plasma sintered Nd-Fe-B magnets were studied. The remanence Br, intrinsic coercivity Hcj, and the maximum energy product（BH）max, of sintered Nd-Fe-B magnets first increase and then decrease with the increase of sintering temperature, TSPS, from 650 °C to 900 °C. The optimal magnetic properties can be obtained when TSPS is 800 °C. The Nd-Fe-B magnet sinter treated at 800 °C was subjected to further hot deformation. Compared with the starting HDDR powders or the SPS treated magnets, the hot-deformed magnets present more obvious anisotropy and possess much better magnetic properties due to the good c-axis texture formed in the deformation process. The anisotropic magnet deformed at 800 °C with 50% compression ratio has a microstructure consisting of well aligned and platelet-shaped Nd2Fe14 B grains without abnormal grain growth and exhibits excellent magnetic properties parallel to the pressing axis.

Constitutive modeling of hot deformation behavior of X20Cr13 martensitic stainless steel with strain effect

Hot deformation behavior ofX20Cr13 martensitic stainless steel was investigated by conducting hot compression tests on Gleeble-1500D thermo-mechanical simulator at the temperature ranging from 1173 to 1423 K and the strain rate ranging from 0.001 to 10 s^-1. The material constants of a and n, activation energy Q and A were calculated as a function of strain by a fifth-order polynomial fit. Constitutive models incorporating deformation temperature, strain rate and strain were developed to model the hot deformation behavior of X20Cr13 martensitic stainless steel based on the Arrhenius equation. The predictable efficiency of the developed constitutive models of X20Cr13 martensitic stainless steel was analyzed by correlation coefficient and average absolute relative error which are 0.996 and 3.22%, respectively.

Hot deformation behavior of homogenized Al-3.2Mg-0.4Er aluminum alloy

The hot deformation behavior of the homogenized Al?3.2Mg?0.4Er aluminum alloy was investigated at 573?723 K under strain rates of 0.001?1 s?1. On the basis of compression experimental results, an accurate phenomenological constitutive equation that coupled the effects of strain rate, deformation temperature and strain was modeled. Furthermore, a kinetic model of dynamic recrystallization and processing map were also presented. The results show that the flow stress of the studied Al?3.2Mg?0.4Er alloy can be predicted accurately using the proposed constitutive model. The evolution of microstructure and the volume fraction of dynamic recrystallization can be described exactly in terms of S-curves with the proposed kinetic model. Moreover, the processing maps for hot working at different strains were constructed, suggesting the optimum processing conditions for this alloy are 573 K, 0.001 s?1 and 723 K, 0.001?0.1 s?1.

Hot deformation behavior and microstructure evolution of 1460 Al-Li alloy

The hot deformation behavior and microstructure evolution of 1460 Al-Li alloy were investigated by isothermal compression test conducted at various strain rates（10-3-10 s-1） and temperatures（573-773 K）. The flow stress curves were corrected by considering the friction at the platen/specimen interface and the temperature change due to the deformation heating. The effects of strain, strain rate and temperature on the deformation behavior were characterized by the Zener-Hollomon parameter in a hyperbolic-sine equation, and the constitutive equations were established according to the peak flow stress associated with dynamic recovery, dynamic recrystallization and the dissolution of T1 phases. In the entire strain rate and temperature range, the prediction capabilities of the developed constitutive equation are proved to be feasible and effective with a linear correlation coefficient and an average absolute relative error coefficient of 0.9909 and 6.72%, respectively.

Hot deformation behavior and microstructural evolution of Al-Zn-Mg-0.25Sc-Zr alloy during compression at elevated temperatures

The hot deformation behavior of Al-Zn-Mg-0.25Sc-Zr alloy and its microstructural evolution were investigated by isothermal axisymmetric hot compression tests at temperatures from 340 to 500°C and strain rates ranging from 0.001 to 10 s -1 .The steady flow stress increased with increasing the strain rate or decreasing the deformation temperature,which can be described by a hyperbolic-sine constitutive equation with the deformation activation energy of 150.25 kJ/mol.The tendency of dynamic recrystallization enhanced at high deforming temperatures and low strain rates,which corresponded to low Z values.With decreasing Z value,the main softening mechanism of the alloy transformed from dynamic recovery to dynamic recrystallization, correspondingly,the subgrain size increased and the dislocation density decreased.